2-溴-6-甲基吡啶-3-甲醛合成路线 （共 2 条）
反应条件
1: With diisobutylaluminium hydride in toluene
T=-50°C; 2.5 h;
2: With sulfuric acid in tetrahydrofuran; toluene
T=20°C; 16 h;
参考文献
Robert, Nicolas; Hoarau, Christophe; Celanire, Sylvain; Ribereau, Pierre; Godard, Alain; Queguiner, Guy; Marsais, Francis
Tetrahedron, 2005 , vol. 61, # 19 p. 4569 - 4576
反应条件
1: 70 percent / Bu4NBr; P2O5 / toluene / 4 h / Heating
2: 77 percent / DIBAL / CH2Cl2 / -78 °C
View Scheme
参考文献
Chelucci, Giorgio; Addis, Daniele; Baldino, Salvatore
Tetrahedron Letters, 2007 , vol. 48, # 19 p. 3359 - 3362
