2,8-二溴-茚并[1,2-b]芴-6,12-二酮合成路线 （共 5 条）
反应条件
sulfuric acid in water
T=120°C; Friedel Crafts Acylation; 10 h; Acidic aqueous solution;
参考文献
NORTHWESTERN UNIVERSITY
Patent: WO2009/17798 A1, 2009 ;
Location in patent: Page/Page column 66 ;
反应条件
sulfuric acid
T=80°C; 12 h;
参考文献
Vak, Doojin; Lim, Bogyu; Lee, Soo-Hyoung; Kim, Dong-Yu
Organic Letters, 2005 , vol. 7, # 19 p. 4229 - 4232
反应条件
1: 93 percent / Pd(PPh3)4; aq. K2CO3 / tetrahydrofuran / 6 h / Heating
2: aq. KMnO4; pyridine / 6 h / Heating
3: H2SO4 / 12 h / 80 °C
View Scheme
参考文献
Vak, Doojin; Lim, Bogyu; Lee, Soo-Hyoung; Kim, Dong-Yu
Organic Letters, 2005 , vol. 7, # 19 p. 4229 - 4232
反应条件
1: 93 percent / Pd(PPh3)4; aq. K2CO3 / tetrahydrofuran / 6 h / Heating
2: aq. KMnO4; pyridine / 6 h / Heating
3: H2SO4 / 12 h / 80 °C
View Scheme
参考文献
Vak, Doojin; Lim, Bogyu; Lee, Soo-Hyoung; Kim, Dong-Yu
Organic Letters, 2005 , vol. 7, # 19 p. 4229 - 4232
反应条件
1: aq. KMnO4; pyridine / 6 h / Heating
2: H2SO4 / 12 h / 80 °C
View Scheme
参考文献
Vak, Doojin; Lim, Bogyu; Lee, Soo-Hyoung; Kim, Dong-Yu
Organic Letters, 2005 , vol. 7, # 19 p. 4229 - 4232
