3,5,5-三甲基-3-(3,5,5-三甲基-2-氧代-吗啉-3-基)吗啉-2-酮合成路线 （共 5 条）
反应条件
2,2',3,3'-tetrahydro-3,3'-dihydroxy-2,2'-dioxo-[3,3'-bi-1H-indole] in dimethylsulfoxide-d6
T=50°C; 65 h; Yield given. Title compound not separated from byproducts;
参考文献
Bennett, Richard W.; Wharry, Donald L.; Koch, Tad H.
Journal of the American Chemical Society, 1980 , vol. 102, # 7 p. 2345 - 2349
参考文献
Burns, John M.; Wharry, Donald L.; Koch, Tad H.
Journal of the American Chemical Society, 1981 , vol. 103, # 4 p. 849 - 856
反应条件
Tris buffer in methanol
T=25°C; Equilibrium constantMechanism;
参考文献
Mahoney, Robert Patrick; Fretwell, Paul A.; Demirdji, Samuel H.; Mauldin III; Benson Jr., Olester; Koch, Tad H.
Journal of the American Chemical Society, 1992 , vol. 114, # 1 p. 186 - 193
反应条件
2,2',3,3'-tetrahydro-3,3'-dihydroxy-2,2'-dioxo-[3,3'-bi-1H-indole] in dimethylsulfoxide-d6
T=50°C; 65 h; Yield given. Title compound not separated from byproducts;
参考文献
Bennett, Richard W.; Wharry, Donald L.; Koch, Tad H.
Journal of the American Chemical Society, 1980 , vol. 102, # 7 p. 2345 - 2349
反应条件
1: CHCl3
2: 80 °C
View Scheme
参考文献
Burns, John M.; Wharry, Donald L.; Koch, Tad H.
Journal of the American Chemical Society, 1981 , vol. 103, # 4 p. 849 - 856
