三(2,6-二甲氧基苯基)磷合成路线 （共 12 条）
反应条件
sodium hydroxide in methanol
参考文献
Wada, Masanori; Kanzaki, Mitsuyuki; Fujiwara, Masanobu; Kajihara, Kazuhisa; Erabi, Tatsuo
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 6 p. 1782 - 1786
反应条件
1: 88 percent / benzene 2: 95 percent / (2,6)3P / methanol / Ambient temperature 3: 95 percent / 1M NaOH / methanol View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 6 p. 1782 - 1786
反应条件
1: 95 percent / (2,6)3P / methanol / Ambient temperature 2: 95 percent / 1M NaOH / methanol View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 6 p. 1782 - 1786
反应条件
1: 95 percent / (2,6)3P / methanol / Ambient temperature 2: 95 percent / 1M NaOH / methanol 3: 95 percent / 12M HCl / butan-2-one 4: 2) 60percent HClO4 / 1) MeOH, 80 deg C, 24 h View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 6 p. 1782 - 1786
反应条件
1: tris(2,6-dimethoxyphenyl)phosphine / methanol / 24 h / Ambient temperature; also with triethylamine, at elevated temperature, and at other concentrations 2: 95 percent / aq. sodium hydroxide / methanol View Scheme
参考文献
Chemistry Letters, , # 6 p. 867 - 870
反应条件
n-butyllithium; phosphorus trichoride 1.) hexane, 42 deg C, 2.) hexane, 42 deg C; Yield given. Multistep reaction;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 14, p. 189 - 210
反应条件
perchloric acid 1) MeOH, 80 deg C, 24 h; Yield given. Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 6 p. 1782 - 1786
反应条件
1: Se / acetone / 3 h / 50 - 60 °C 2: methanol / 8 h / Ambient temperature 3: aq. NaOH View Scheme
参考文献
Wada, Masanori; Hayase, Shuichi; Fujiwara, Masanobu; Kawaguchi, Tetsuji; Iwasaki, Toshio; Uo, Akira; Erabi, Tatsuo
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 3 p. 655 - 664
反应条件
dihydrogen peroxide in tetrahydrofuran; water 0.533333 h;
参考文献
Denton, Ross M.; An, Jie; Adeniran, Beatrice; Blake, Alexander J.; Lewis, William; Poulton, Andrew M.
Journal of Organic Chemistry, 2011 , vol. 76, # 16 p. 6749 - 6767
反应条件
hydrogenchloride in butanone
参考文献
Wada, Masanori; Kanzaki, Mitsuyuki; Fujiwara, Masanobu; Kajihara, Kazuhisa; Erabi, Tatsuo
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 6 p. 1782 - 1786
