6-溴-3,4-二氢喹喔啉-2(1H)-酮合成路线 （共 3 条）
反应条件
sodium carbonate; sodium iodide in acetonitrile
Inert atmosphereReflux;
参考文献
Universitat des Saarlandes
Patent: US2011/112067 A1, 2011 ;
Location in patent: Page/Page column 33 ;
US 20110112067 A1
反应条件
1.1: 1.5 h / Inert atmosphere; Reflux
2.1: acetic acid; ammonium chloride; iron / N,N-dimethyl-formamide; water / 0.5 h / 50 °C
2.2: pH 9
3.1: sodium carbonate / sodium iodide / acetonitrile / Reflux; Inert atmosphere
View Scheme
参考文献
Universitat des Saarlandes
Patent: US2011/112067 A1, 2011 ;
US 20110112067 A1
反应条件
1.1: acetic acid; ammonium chloride; iron / N,N-dimethyl-formamide; water / 0.5 h / 50 °C
1.2: pH 9
2.1: sodium carbonate / sodium iodide / acetonitrile / Reflux; Inert atmosphere
View Scheme
参考文献
Universitat des Saarlandes
Patent: US2011/112067 A1, 2011 ;
US 20110112067 A1
