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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
855242-15-8
合成路线
（共 14 条）
1357024-84-0
+
77-78-1
硫酸二甲酯
→
反应条件
855242-15-8
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C; 6 h;
参考文献
Huang, Guan-Jhong; Bhaskar Reddy, M. Vijaya; Kuo, Ping-Chung; Huang, Chieh-Hung; Shih, Hung-Cheng; Lee, E.-Jian; Yang, Mei-Lin; Leu, Yann-Lii; Wu, Tian-Shung
European Journal of Medicinal Chemistry, 2012 , vol. 48, p. 371 - 378
→
反应条件
855242-15-8
反应条件
potassium carbonate in acetone
参考文献
Huang, Guan-Jhong; Bhaskar Reddy, M. Vijaya; Kuo, Ping-Chung; Huang, Chieh-Hung; Shih, Hung-Cheng; Lee, E.-Jian; Yang, Mei-Lin; Leu, Yann-Lii; Wu, Tian-Shung
European Journal of Medicinal Chemistry, 2012 , vol. 48, p. 371 - 378
858218-65-2
+
77-78-1
硫酸二甲酯
→
反应条件
855242-15-8
反应条件
sodium hydroxide in water
参考文献
Su, Chung-Ren; Shen, Yuh-Chiang; Kuo, Ping-Chung; Leu, Yann-Lii; Damu, Amooru G.; Wang, Yea-Hwey; Wu, Tian-Shung
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 24 p. 6155 - 6160
708-76-9
4,6-二甲氧基水杨醛
→
反应条件
855242-15-8
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 8 h / 80 °C 2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C 3: sodium hydroxide / methanol / 3 h / 20 °C 4: potassium carbonate / N,N-dimethyl-formamide / 6 h / 80 °C View Scheme
参考文献
Huang, Guan-Jhong; Bhaskar Reddy, M. Vijaya; Kuo, Ping-Chung; Huang, Chieh-Hung; Shih, Hung-Cheng; Lee, E.-Jian; Yang, Mei-Lin; Leu, Yann-Lii; Wu, Tian-Shung
European Journal of Medicinal Chemistry, 2012 , vol. 48, p. 371 - 378
54917-02-1
→
反应条件
855242-15-8
反应条件
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C 2: sodium hydroxide / methanol / 3 h / 20 °C 3: potassium carbonate / N,N-dimethyl-formamide / 6 h / 80 °C View Scheme
参考文献
Huang, Guan-Jhong; Bhaskar Reddy, M. Vijaya; Kuo, Ping-Chung; Huang, Chieh-Hung; Shih, Hung-Cheng; Lee, E.-Jian; Yang, Mei-Lin; Leu, Yann-Lii; Wu, Tian-Shung
European Journal of Medicinal Chemistry, 2012 , vol. 48, p. 371 - 378
830-79-5
2,4,6-三甲氧基苯甲醛
→
反应条件
855242-15-8
反应条件
1.1: boron tribromide / dichloromethane / -78 - 20 °C 1.2: Cooling with ice 2.1: potassium carbonate / N,N-dimethyl-formamide / 8 h / 80 °C 3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C 4.1: sodium hydroxide / methanol / 3 h / 20 °C 5.1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 80 °C View Scheme
参考文献
Huang, Guan-Jhong; Bhaskar Reddy, M. Vijaya; Kuo, Ping-Chung; Huang, Chieh-Hung; Shih, Hung-Cheng; Lee, E.-Jian; Yang, Mei-Lin; Leu, Yann-Lii; Wu, Tian-Shung
European Journal of Medicinal Chemistry, 2012 , vol. 48, p. 371 - 378
3934-87-0
3,4-二羟基-5-甲氧基苯甲醛
→
反应条件
855242-15-8
反应条件
1: sodium carbonate / acetone / 6 h / Reflux 2: potassium carbonate / N,N-dimethyl-formamide / 6 h / 80 °C 3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C 4: sodium hydroxide / methanol / 3 h / 20 °C 5: potassium carbonate / acetone View Scheme
参考文献
Huang, Guan-Jhong; Bhaskar Reddy, M. Vijaya; Kuo, Ping-Chung; Huang, Chieh-Hung; Shih, Hung-Cheng; Lee, E.-Jian; Yang, Mei-Lin; Leu, Yann-Lii; Wu, Tian-Shung
European Journal of Medicinal Chemistry, 2012 , vol. 48, p. 371 - 378
2973-76-4
5-溴香兰素
→
反应条件
855242-15-8
反应条件
1.1: copper; sodium hydroxide / water / Reflux 1.2: Reflux 2.1: sodium carbonate / acetone / 6 h / Reflux 3.1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 80 °C 4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C 5.1: sodium hydroxide / methanol / 3 h / 20 °C 6.1: potassium carbonate / acetone View Scheme
参考文献
Huang, Guan-Jhong; Bhaskar Reddy, M. Vijaya; Kuo, Ping-Chung; Huang, Chieh-Hung; Shih, Hung-Cheng; Lee, E.-Jian; Yang, Mei-Lin; Leu, Yann-Lii; Wu, Tian-Shung
European Journal of Medicinal Chemistry, 2012 , vol. 48, p. 371 - 378
29865-90-5
3,4-二甲氧基-5-羟基苯甲醛
→
反应条件
855242-15-8
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 80 °C 2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C 3: sodium hydroxide / methanol / 3 h / 20 °C 4: potassium carbonate / acetone View Scheme
参考文献
Huang, Guan-Jhong; Bhaskar Reddy, M. Vijaya; Kuo, Ping-Chung; Huang, Chieh-Hung; Shih, Hung-Cheng; Lee, E.-Jian; Yang, Mei-Lin; Leu, Yann-Lii; Wu, Tian-Shung
European Journal of Medicinal Chemistry, 2012 , vol. 48, p. 371 - 378
57230-04-3
→
反应条件
855242-15-8
反应条件
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C 2: sodium hydroxide / methanol / 3 h / 20 °C 3: potassium carbonate / acetone View Scheme
参考文献
Huang, Guan-Jhong; Bhaskar Reddy, M. Vijaya; Kuo, Ping-Chung; Huang, Chieh-Hung; Shih, Hung-Cheng; Lee, E.-Jian; Yang, Mei-Lin; Leu, Yann-Lii; Wu, Tian-Shung
European Journal of Medicinal Chemistry, 2012 , vol. 48, p. 371 - 378
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