1: With lithium hexamethyldisilazane in tetrahydrofuran
T=-78°C; Metallation; 0.25 h;
2: With copper(ll) bromide in tetrahydrofuran
T=-78 - 20°C; Dimerization; bromination; Title compound not separated from byproducts;
参考文献
Falcou, Aurelie; Boullais, Claude
Journal of Labelled Compounds and Radiopharmaceuticals, 1998 , vol. 41, # 7 p. 657 - 668