2,3,4-三-O-苯甲酰基-6-脱氧-L-古洛吡喃糖基溴化物合成路线 （共 3 条）
反应条件
1: boron trifluoride diethyl etherate / dichloromethane / 8 h / 0 - 20 °C
2: N-bromosuccinmide / acetone; water / 1 h / -25 °C
View Scheme
参考文献
Wang, Ying-Hsin; Yeh, Hsien-Wei; Wang, Hsiao-Wen; Yu, Chia-Chun; Guh, Jih-Hwa; Liu, Der-Zen; Liang, Pi-Hui
Carbohydrate Research, 2013 , vol. 375, p. 118 - 135
反应条件
1: pyridine; 4-(N,N-dimethlyamino)pyridine / 5 h / 0 - 20 °C
2: boron trifluoride diethyl etherate / dichloromethane / 8 h / 0 - 20 °C
3: N-bromosuccinmide / acetone; water / 1 h / -25 °C
View Scheme
参考文献
Wang, Ying-Hsin; Yeh, Hsien-Wei; Wang, Hsiao-Wen; Yu, Chia-Chun; Guh, Jih-Hwa; Liu, Der-Zen; Liang, Pi-Hui
Carbohydrate Research, 2013 , vol. 375, p. 118 - 135
反应条件
1: pyridine; 4-(N,N-dimethlyamino)pyridine / 5 h / 0 - 20 °C
2: boron trifluoride diethyl etherate / dichloromethane / 8 h / 0 - 20 °C
3: N-bromosuccinmide / acetone; water / 1 h / -25 °C
View Scheme
参考文献
Wang, Ying-Hsin; Yeh, Hsien-Wei; Wang, Hsiao-Wen; Yu, Chia-Chun; Guh, Jih-Hwa; Liu, Der-Zen; Liang, Pi-Hui
Carbohydrate Research, 2013 , vol. 375, p. 118 - 135
