2,9-二丁基-1,10-邻二氮杂菲合成路线 （共 4 条）
反应条件
1: in hexane; toluene T=0 - 25°C; Inert atmosphereSchlenk techniqueGlovebox; 2: With manganese(IV) oxide in toluene 6 h; Inert atmosphereSchlenk techniqueGlovebox;
参考文献
Wang, Tianli; Chen, Fei; Qin, Jie; He, Yan-Mei; Fan, Qing-Hua
Angewandte Chemie - International Edition, 2013 , vol. 52, # 28 p. 7172 - 7176
Angew. Chem., 2013 , vol. 125, # 28 p. 7313 - 7317
反应条件
potassium permanganate 1.) benzene/hexane, 3 h, 0 deg C; 2.) acetone; Yield given. Multistep reaction;
参考文献
Pijper; Van der Goot; Timmerman; Nauta Th.
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 5 p. 399 - 404
反应条件
potassium permanganate 1.) benzene/hexane, 3 h, 0 deg C; 2.) acetone; Yield given. Multistep reaction;
参考文献
Pijper; Van der Goot; Timmerman; Nauta Th.
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 5 p. 399 - 404
反应条件
sulfuric acid; nitric acid; potassium bromide in water
2 h; Heating;
参考文献
Ott, Sascha; Faust, Ruediger
Synthesis, 2005 , # 18 art. no. T01905SS, p. 3135 - 3139
