(3-((叔丁基二苯基甲硅烷基)氧基)苯基)硼酸合成路线 （共 3 条）
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 2 h;
2: With boric acid trimethyl ester in tetrahydrofuran; hexane
T=-78°C; 2 h;
参考文献
Sato, Hiroshi; Tashiro, Kentaro; Shinmori, Hideyuki; Osuka, Atsuhiro; Aida, Takuzo
Chemical Communications, 2005 , # 18 p. 2324 - 2326
反应条件
1.1: 98 percent / imidazole / dimethylformamide / 2 h / 20 °C
2.1: BuLi / tetrahydrofuran; hexane / 2 h / -78 °C
2.2: 53 percent / B(OMe)3 / tetrahydrofuran; hexane / 2 h / -78 °C
View Scheme
参考文献
Sato, Hiroshi; Tashiro, Kentaro; Shinmori, Hideyuki; Osuka, Atsuhiro; Aida, Takuzo
Chemical Communications, 2005 , # 18 p. 2324 - 2326
反应条件
1.1: 98 percent / imidazole / dimethylformamide / 2 h / 20 °C
2.1: BuLi / tetrahydrofuran; hexane / 2 h / -78 °C
2.2: 53 percent / B(OMe)3 / tetrahydrofuran; hexane / 2 h / -78 °C
View Scheme
参考文献
Sato, Hiroshi; Tashiro, Kentaro; Shinmori, Hideyuki; Osuka, Atsuhiro; Aida, Takuzo
Chemical Communications, 2005 , # 18 p. 2324 - 2326
