1,7-(二氧杂)-2,6-二氮杂-4,7a-二硫杂-3H,5H-苯并(cd)并环戊二烯-4-氧化物合成路线 （共 4 条）
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
0.25 h; Ambient temperature;
参考文献
Camilleri, Patrick; Clark, Michael T.; Gilmore, Ian J.; Cole-Hamilton, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 833 - 836
反应条件
1: NH2OH*HCl; NaOAc*H2O / ethanol; H2O / 0.5 h
2: 46 percent / SCl2; iodine / tetrahydrofuran / -70 - -40 °C
3: 70 percent / m-chloroperbenzoic acid / CH2Cl2 / 0.25 h / Ambient temperature
View Scheme
参考文献
Camilleri, Patrick; Clark, Michael T.; Gilmore, Ian J.; Cole-Hamilton, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 833 - 836
反应条件
1: 60percent NaH / toluene; tetrahydrofuran / Ambient temperature
2: NH2OH*HCl; NaOAc*H2O / ethanol; H2O / 0.5 h
3: 46 percent / SCl2; iodine / tetrahydrofuran / -70 - -40 °C
4: 70 percent / m-chloroperbenzoic acid / CH2Cl2 / 0.25 h / Ambient temperature
View Scheme
参考文献
Camilleri, Patrick; Clark, Michael T.; Gilmore, Ian J.; Cole-Hamilton, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 833 - 836
反应条件
1: 46 percent / SCl2; iodine / tetrahydrofuran / -70 - -40 °C
2: 70 percent / m-chloroperbenzoic acid / CH2Cl2 / 0.25 h / Ambient temperature
View Scheme
参考文献
Camilleri, Patrick; Clark, Michael T.; Gilmore, Ian J.; Cole-Hamilton, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 833 - 836
