4-溴-3-羟基甲基-1-氧基-2,2,5,5-四甲基-delta3-吡咯啉合成路线 (共 4 条)
反应条件
sodium tetrahydroborate; sodium hydrogencarbonate in 1,4-dioxane
T=20°C; 4 h;
参考文献
Chudinov, A. V.; Rozantsev, E. G.; Rozynov, B. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 2 p. 370 - 375
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 2 p. 409 - 413
反应条件
sodium tetrahydroborate in ethanol
2 h;
参考文献
Chudinov, A. V.; Rozantsev, E. G.; Rozynov, B. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 2 p. 370 - 375
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 2 p. 409 - 413
反应条件
aluminum oxide in benzene
T=20°C; 5 h;
参考文献
Chudinov, A. V.; Rozantsev, E. G.; Rozynov, B. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 2 p. 370 - 375
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 2 p. 409 - 413
反应条件
1: 90 percent / CrO3, pyridine / CH2Cl2 / 0.25 h
2: 22.8 percent / Al2O3 / benzene / 5 h / 20 °C
View Scheme
参考文献
Chudinov, A. V.; Rozantsev, E. G.; Rozynov, B. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 2 p. 370 - 375
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 2 p. 409 - 413