1-(2-苯并呋喃基)-1-丁酮合成路线 （共 3 条）
反应条件
titanium tetrachloride in dichloromethane
T=-78°C; 0.0833333 h;
参考文献
Gill, Melvyn
Tetrahedron, 1984 , vol. 40, # 3 p. 621 - 626
反应条件
1: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 1 h; 2.) -78 deg C, 1 h; room temp., overnight
2: 92 percent / titanium(IV) chloride / CH2Cl2 / 0.08 h / -78 °C
View Scheme
参考文献
Gill, Melvyn
Tetrahedron, 1984 , vol. 40, # 3 p. 621 - 626
反应条件
1: (benzofuran-2-yl)methylketone With lithium diisopropyl amide in tetrahydrofuran
T=-78°C; 1 h; Inert atmosphere;
2: ethyl iodide in tetrahydrofuran
24 h;
参考文献
Park, Soohyun; Kim, Sang Jun; Hyun, Myung Ho
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 10 p. 3497 - 3500
