1-甲基-2-亚甲基环戊烷e羰基氯化物合成路线 （共 9 条）
反应条件
thionyl chloride
T=120°C; 0.833333 h;
参考文献
Karpf, Martin
Helvetica Chimica Acta, 1984 , vol. 67, # 1 p. 73 - 85
反应条件
1: 87 percent / tetrahydrofuran / 2 h / Ambient temperature
2: 88 percent / KOH / methanol; H2O / 24 h / Ambient temperature
3: 93 percent / SOCl2 / 0.83 h / 120 °C
View Scheme
参考文献
Karpf, Martin
Helvetica Chimica Acta, 1984 , vol. 67, # 1 p. 73 - 85
反应条件
1: 88 percent / KOH / methanol; H2O / 24 h / Ambient temperature
2: 93 percent / SOCl2 / 0.83 h / 120 °C
View Scheme
参考文献
Karpf, Martin
Helvetica Chimica Acta, 1984 , vol. 67, # 1 p. 73 - 85
反应条件
aluminium trichloride in dichloromethane
T=-30°C; 1 h;
参考文献
Karpf, Martin
Helvetica Chimica Acta, 1984 , vol. 67, # 1 p. 73 - 85
反应条件
aluminium trichloride in dichloromethane
T=-30°C; 1 h;
参考文献
Karpf, Martin
Helvetica Chimica Acta, 1984 , vol. 67, # 1 p. 73 - 85
反应条件
aluminium trichloride
参考文献
Karpf, Martin
Helvetica Chimica Acta, 1984 , vol. 67, # 1 p. 73 - 85
反应条件
aluminium trichloride in dichloromethane
T=-30°C; 1 h;
参考文献
Karpf, Martin
Helvetica Chimica Acta, 1984 , vol. 67, # 1 p. 73 - 85
反应条件
1: 57 percent / AlCl3 / CH2Cl2 / 1 h / -30 °C
2: 82 percent / HCl / CHCl3 / 20 h / Ambient temperature
View Scheme
参考文献
Karpf, Martin
Helvetica Chimica Acta, 1984 , vol. 67, # 1 p. 73 - 85
反应条件
aluminium trichloride in dichloromethane
T=-30°C; 1 h;
参考文献
Karpf, Martin
Helvetica Chimica Acta, 1984 , vol. 67, # 1 p. 73 - 85
