in neat (no solvent, solid phase) byproducts: cis-1,2-bis(thiomethoxyl)ethylene, trans-1,2-bis(thiomethoxyl)ethylene, tris(thiomethoxyl)methane; complex sealed in ampule under N2, heated at 200°C for 2 min; extd. (CCl4) at room temp., not isolated, detected by mass spectroscopy;