(9H-芴-9-基)甲基 烯丙基氨基甲酸酯合成路线 (共 2 条)
反应条件
1: With ozone in methanol; dichloromethane T=-78°C; 0.0833333 h; Inert atmosphere; 2: With dimethylsulfide in methanol; dichloromethane T=-78 - 22°C; 4 h; Inert atmosphere;
参考文献
Mszar, Nicholas W.; Haeffner, Fredrik; Hoveyda, Amir H.
Journal of the American Chemical Society, 2014 , vol. 136, # 9 p. 3362 - 3365
反应条件
sodium hydrogencarbonate in 1,4-dioxane
T=0 - 20°C; 23 h; Inert atmosphere;
参考文献
Eto, Kohei; Yoshino, Madoka; Takahashi, Keisuke; Ishihara, Jun; Hatakeyama, Susumi
Organic Letters, 2011 , vol. 13, # 19 p. 5398 - 5401