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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
85654-22-4
合成路线
（共 12 条）
929859-22-3
→
反应条件
85654-22-4
反应条件
palladium 10 on activated carbon; hydrogen in ethanol T=20°C; Inert atmosphere;
参考文献
Darras, Fouad H.; Pockes, Steffen; Huang, Guozheng; Wehle, Sarah; Strasser, Andrea; Wittmann, Hans-Joachim; Nimczick, Martin; Sotriffer, Christoph A.; Decker, Michael
ACS Chemical Neuroscience, 2014 , vol. 5, # 3 p. 225 - 242
616-45-5
2-吡咯烷酮
+
195986-91-5
5-羟基靛红酸酐
→
反应条件
85654-22-4
反应条件
T=130°C; P=2585.81 - 5171.62 Torr; 1 h; Sealed tube;
参考文献
Darras, Fouad H.; Kling, Beata; Heilmann, Joerg; Decker, Michael
ACS Medicinal Chemistry Letters, 2012 , vol. 3, # 11 p. 914 - 919
616-45-5
2-吡咯烷酮
+
394-31-0
2-氨基-5-羟基苯甲酸
→
反应条件
85654-22-4
反应条件
thionyl chloride in benzene 4 h; Reflux;
参考文献
Jahng, Katherine Chae; Kim, Seung Ill; Kim, Dong Hyeon; Seo, Chang Seob; Son, Jong-Keun; Lee, Seung Ho; Lee, Eung Seok; Jahng, Yurngdong
Chemical and Pharmaceutical Bulletin, 2008 , vol. 56, # 4 p. 607 - 609
622829-44-1
→
反应条件
85654-22-4
反应条件
1: potassium hydroxide / methanol; water / 2 h / |Reflux 2: oxalyl dichloride / tetrahydrofuran / 2 h / |Reflux 3: 1 h / 2585.81 - 5171.62 Torr / |Microwave irradiation; |Heating 4: palladium 10 on activated carbon; hydrogen / ethanol / 20 °C / |Inert atmosphere View Scheme
参考文献
Darras, Fouad H.; Pockes, Steffen; Huang, Guozheng; Wehle, Sarah; Strasser, Andrea; Wittmann, Hans-Joachim; Nimczick, Martin; Sotriffer, Christoph A.; Decker, Michael
ACS Chemical Neuroscience, 2014 , vol. 5, # 3 p. 225 - 242
394-31-0
2-氨基-5-羟基苯甲酸
→
反应条件
85654-22-4
反应条件
1: 1,4-dioxane / 2 h / |Reflux 2: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C / |Inert atmosphere 3: potassium hydroxide / methanol; water / 2 h / |Reflux 4: oxalyl dichloride / tetrahydrofuran / 2 h / |Reflux 5: 1 h / 2585.81 - 5171.62 Torr / |Microwave irradiation; |Heating 6: palladium 10 on activated carbon; hydrogen / ethanol / 20 °C / |Inert atmosphere View Scheme
参考文献
Darras, Fouad H.; Pockes, Steffen; Huang, Guozheng; Wehle, Sarah; Strasser, Andrea; Wittmann, Hans-Joachim; Nimczick, Martin; Sotriffer, Christoph A.; Decker, Michael
ACS Chemical Neuroscience, 2014 , vol. 5, # 3 p. 225 - 242
104356-42-5
→
反应条件
85654-22-4
反应条件
1: oxalyl dichloride / tetrahydrofuran / 2 h / |Reflux 2: 1 h / 2585.81 - 5171.62 Torr / |Microwave irradiation; |Heating 3: palladium 10 on activated carbon; hydrogen / ethanol / 20 °C / |Inert atmosphere View Scheme
参考文献
Darras, Fouad H.; Pockes, Steffen; Huang, Guozheng; Wehle, Sarah; Strasser, Andrea; Wittmann, Hans-Joachim; Nimczick, Martin; Sotriffer, Christoph A.; Decker, Michael
ACS Chemical Neuroscience, 2014 , vol. 5, # 3 p. 225 - 242
567-62-4
6-羟基邻氨基苯甲酸
→
反应条件
85654-22-4
反应条件
1: tetrahydrofuran / 3 h / 40 - 50 °C 2: 1 h / 130 °C / 2585.81 - 5171.62 Torr / |Sealed tube View Scheme
参考文献
Darras, Fouad H.; Kling, Beata; Heilmann, Joerg; Decker, Michael
ACS Medicinal Chemistry Letters, 2012 , vol. 3, # 11 p. 914 - 919
60811-32-7
→
反应条件
85654-22-4
反应条件
potassium hydroxide; hydrogen bromide 1) reflux, 5 h; Yield given. Multistep reaction;
参考文献
Karimov, A.; Telezhenetskaya, M. V.; Yunusov, S. Yu.
Chemistry of Natural Compounds, 1982 , vol. 18, # 4 p. 466 - 472
Khimiya Prirodnykh Soedinenii, 1982 , vol. 18, # 4 p. 498 - 504
39755-95-8
5-甲氧基靛红
→
反应条件
85654-22-4
反应条件
1: 1) 30percent H2O2, 5percent aq. NaOH; 2) conc. HCl 2: 50 percent / POCl3 / 1 h / Heating 3: 1) 47percent HBr, 2) 10percent KOH / 1) reflux, 5 h View Scheme
参考文献
Karimov, A.; Telezhenetskaya, M. V.; Yunusov, S. Yu.
Chemistry of Natural Compounds, 1982 , vol. 18, # 4 p. 466 - 472
Khimiya Prirodnykh Soedinenii, 1982 , vol. 18, # 4 p. 498 - 504
6335-41-7
(2Z)-2-羟基亚胺-N-(4-甲氧基苯基)乙酰胺
→
反应条件
85654-22-4
反应条件
1: 67.7 percent / 90percent H2SO4 / 0.5 h / 70 °C 2: 1) 30percent H2O2, 5percent aq. NaOH; 2) conc. HCl 3: 50 percent / POCl3 / 1 h / Heating 4: 1) 47percent HBr, 2) 10percent KOH / 1) reflux, 5 h View Scheme
参考文献
Karimov, A.; Telezhenetskaya, M. V.; Yunusov, S. Yu.
Chemistry of Natural Compounds, 1982 , vol. 18, # 4 p. 466 - 472
Khimiya Prirodnykh Soedinenii, 1982 , vol. 18, # 4 p. 498 - 504
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