in neat (no solvent)
byproducts: hydrogen; introduction of EtNH2*BH3 under N2 into flask; heating in an oil bath byslow raising the temp. to 120°C for 30 min; heating at this temp . for 1 h; heating at 200°C for 1 h; distn. in vac.;
Mikhailov, B. M.; Dorokhov, V. A.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1961 , p. 1346 - 1348
Show Details
Gmelin Handbook: B: B-Verb.4, 13.3.1, page 325 - 329
