3-[4-(二甲基氨基)苯基]-1-丙醇合成路线 （共 5 条）
反应条件
potassium hydroxide; isopropyl alcohol; PdMCM-41
5 h;
参考文献
Selvam, Parasuraman; Sonavane, Sachin U.; Mohapatra, Susanta K.; Jayaram, Radha V.
Tetrahedron Letters, 2004 , vol. 45, # 15 p. 3071 - 3075
反应条件
lithium aluminium tetrahydride in diethyl ether
1 h;
参考文献
Borovkov, V. V.; Evstigneeva, R. P.; Gribkov, A. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1995 , vol. 31, # 3 p. 296 - 302
Khimiya Geterotsiklicheskikh Soedinenii, 1995 , # 3 p. 343 - 350
反应条件
1: 56 percent / H2 / 10percentPd/C / tetrahydrofuran / 36 h
2: 38 percent / lithium aluminum hydrate / diethyl ether / 1 h
View Scheme
参考文献
Borovkov, V. V.; Evstigneeva, R. P.; Gribkov, A. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1995 , vol. 31, # 3 p. 296 - 302
Khimiya Geterotsiklicheskikh Soedinenii, 1995 , # 3 p. 343 - 350
反应条件
1: 100 percent / diethyl ether; ethanol; H2O / 1 h / 0 °C
2: 56 percent / H2 / 10percentPd/C / tetrahydrofuran / 36 h
3: 38 percent / lithium aluminum hydrate / diethyl ether / 1 h
View Scheme
参考文献
Borovkov, V. V.; Evstigneeva, R. P.; Gribkov, A. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1995 , vol. 31, # 3 p. 296 - 302
Khimiya Geterotsiklicheskikh Soedinenii, 1995 , # 3 p. 343 - 350
反应条件
3: H2 / Pd/C
4: LiAlH4
View Scheme
参考文献
Borovkov, V. V.; Evstigneeva, R. P.; Filippovich, E. I.; Rozynov, B. V.
Doklady Chemistry, 1989 , vol. 308, # 4-6 p. 275 - 279
Dokl. Akad. Nauk SSSR Ser. Khim., 1989 , vol. 308, # 4 p. 874 - 878
