2-异硫氰基-4,5,6,7-四氢-1-苯并噻吩-3-羧酸乙酯合成路线 （共 6 条）
反应条件
water; sodium hydrogencarbonate in chloroform 0.5 h; Ambient temperature;
参考文献
Granata, Giuseppe; Barbagallo, Salvatore; Perdicaro, Antonio; Marrazzo, Agostino; Santagati, Andrea; Lombardo, Laura; Cardile, Venera
Journal of Heterocyclic Chemistry, 2006 , vol. 43, # 4 p. 1099 - 1104
反应条件
1: acetone / 20 °C 2: bis(trichloromethyl) carbonate / chloroform / 4.5 h / 0 - 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 43, # 24 p. 3342 - 3351
反应条件
in dichloromethane; acetonitrile Aza-Wittig reaction; 24 h; Inert atmosphereReflux;
参考文献
Synthetic Communications, , vol. 40, # 10 p. 1453 - 1460
反应条件
ammonia in dichloromethane 3 h; Ambient temperature;
参考文献
Leistner, Siegfried; Guetschow, Michael; Wagner, Guenther
Synthesis, 1987 , # 5 p. 466 - 470
反应条件
1: 40 percent / hydrazine hydrate / benzene / 8 h / Heating
2: 60 percent / phosphorus pentoxide, methanesulfonic acid / 9 h / 80 °C
View Scheme
参考文献
Santagati, Andrea; Santagati, Maria; Modica, Maria
Heterocycles, 1993 , vol. 36, # 6 p. 1315 - 1321
参考文献
Chumakova; Demchenko; Krasovsky; Dolishnyak; Lozinskii
Chemistry of Heterocyclic Compounds, 2003 , vol. 39, # 8 p. 1002 - 1012
