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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
85732-37-2
合成路线
（共 8 条）
85732-38-3
→
反应条件
85732-37-2
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in methanol; water T=40°C; 20 h;
参考文献
Takai; Obase; Teranishi; Karasawa; Kubo; Shuto; Kasuya; Hashikami; Karashima; Shigenobu
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 3 p. 1129 - 1139
3612-20-2
N-苄基哌啶酮
→
反应条件
85732-37-2
反应条件
1: 45.4 percent / n-butyllithium / hexane; tetrahydrofuran / -5 °C 2: 62.4 percent / 3 N H2SO4 / H2O / 16 h / Heating 3: pyridine / 0 °C 4: aq. NaOH / methanol 5: 85.5 percent / hydrogen, 1N HCl / 10percent Pd-C / H2O; methanol / 20 h / 40 °C View Scheme
参考文献
Takai; Obase; Teranishi; Karasawa; Kubo; Shuto; Kasuya; Hashikami; Karashima; Shigenobu
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 3 p. 1129 - 1139
65854-91-3
4'-氯代新戊酰苯胺
→
反应条件
85732-37-2
反应条件
1: 45.4 percent / n-butyllithium / hexane; tetrahydrofuran / -5 °C 2: 62.4 percent / 3 N H2SO4 / H2O / 16 h / Heating 3: pyridine / 0 °C 4: aq. NaOH / methanol 5: 85.5 percent / hydrogen, 1N HCl / 10percent Pd-C / H2O; methanol / 20 h / 40 °C View Scheme
参考文献
Takai; Obase; Teranishi; Karasawa; Kubo; Shuto; Kasuya; Hashikami; Karashima; Shigenobu
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 3 p. 1129 - 1139
85732-68-9
→
反应条件
85732-37-2
反应条件
1: 62.4 percent / 3 N H2SO4 / H2O / 16 h / Heating 2: pyridine / 0 °C 3: aq. NaOH / methanol 4: 85.5 percent / hydrogen, 1N HCl / 10percent Pd-C / H2O; methanol / 20 h / 40 °C View Scheme
参考文献
Takai; Obase; Teranishi; Karasawa; Kubo; Shuto; Kasuya; Hashikami; Karashima; Shigenobu
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 3 p. 1129 - 1139
85732-70-3
→
反应条件
85732-37-2
反应条件
1: pyridine / 0 °C 2: aq. NaOH / methanol 3: 85.5 percent / hydrogen, 1N HCl / 10percent Pd-C / H2O; methanol / 20 h / 40 °C View Scheme
参考文献
Takai; Obase; Teranishi; Karasawa; Kubo; Shuto; Kasuya; Hashikami; Karashima; Shigenobu
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 3 p. 1129 - 1139
98203-36-2
→
反应条件
85732-37-2
反应条件
1: aq. NaOH / methanol 2: 85.5 percent / hydrogen, 1N HCl / 10percent Pd-C / H2O; methanol / 20 h / 40 °C View Scheme
参考文献
Takai; Obase; Teranishi; Karasawa; Kubo; Shuto; Kasuya; Hashikami; Karashima; Shigenobu
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 3 p. 1129 - 1139
85732-37-2
→
反应条件
84060-24-2
反应条件
1: 86.3 percent / TEA / ethanol / Ambient temperature 2: 97.7 percent / NaBH4 / ethanol / 72 h / Ambient temperature View Scheme
参考文献
Takai; Obase; Teranishi; Karasawa; Kubo; Shuto; Kasuya; Hashikami; Karashima; Shigenobu
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 3 p. 1129 - 1139
85732-37-2
→
反应条件
85732-25-8
反应条件
1: 93.2 percent / TEA / ethanol / Ambient temperature 2: 91.9 percent / NaBH4 / ethanol / 72 h / Ambient temperature View Scheme
参考文献
Takai; Obase; Teranishi; Karasawa; Kubo; Shuto; Kasuya; Hashikami; Karashima; Shigenobu
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 3 p. 1129 - 1139
