6,7,12,13-四氢-5H-吲哚并[2,3-a]吡咯并[3,4-c]咔唑-5-酮合成路线 （共 45 条）
反应条件
1: 15 percent / Cu(OAc)2; air / Pd(OAc)2 / toluene / 12 h / 760 Torr / Heating 2: 71 percent / AlCl3 / methoxybenzene / 1 h / 110 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 72, # 6 p. 2008 - 2014
反应条件
1: 50 percent / Cu(OAc)2; air / Pd(OAc)2 / dimethylsulfoxide / 12 h / 110 °C / 760 Torr 2: 99 percent / AlCl3 / methoxybenzene / 1 h / 110 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 72, # 6 p. 2008 - 2014
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C; 0.166667 h;
参考文献
European Journal of Organic Chemistry, , # 7 p. 1303 - 1310
反应条件
triphenylphosphine 1.5 h; Heating;
参考文献
Moody, Christopher J.; Rahimtoola, Kulsum F.; Porter, Barry; Ross, Barry C.
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2105 - 2114
反应条件
benzenesulfonamide; NADH-H+; octadecyl-trimethylammonium chloride; StaP in various solvent(s) pH=8.0; Enzyme kinetics; Further Variations:Reagents;
参考文献
Journal of the American Chemical Society, , vol. 128, # 37 p. 12289 - 12298
反应条件
1: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / tetrachloromethane / 4 h / Inert atmosphere; Reflux 2: ammonia / tetrahydrofuran; water / 2 h / Reflux; Inert atmosphere 3: triethyl phosphite / 1,2-dichloro-benzene / 12 h / Reflux; Inert atmosphere 4: methanol; potassium carbonate / tetrahydrofuran / 10 h / Inert atmosphere; Reflux View Scheme
参考文献
Organic Letters, , vol. 13, # 6 p. 1418 - 1421
反应条件
1: ammonia / tetrahydrofuran; water / 2 h / Reflux; Inert atmosphere 2: triethyl phosphite / 1,2-dichloro-benzene / 12 h / Reflux; Inert atmosphere 3: methanol; potassium carbonate / tetrahydrofuran / 10 h / Inert atmosphere; Reflux View Scheme
参考文献
Organic Letters, , vol. 13, # 6 p. 1418 - 1421
反应条件
1: triethyl phosphite / 1,2-dichloro-benzene / 12 h / Reflux; Inert atmosphere 2: methanol; potassium carbonate / tetrahydrofuran / 10 h / Inert atmosphere; Reflux View Scheme
参考文献
Organic Letters, , vol. 13, # 6 p. 1418 - 1421
反应条件
in methanol; dimethyl sulfoxide Irradiation;
参考文献
Gaudencio, Susana P.; Santos, Maria M. M.; Lobo, Ana M.; Prabhakar, Sundaresan
Tetrahedron Letters, 2003 , vol. 44, # 12 p. 2577 - 2578
反应条件
1: 71 percent / Ph3P, diethyl azodicarboxylate / tetrahydrofuran / 26 h / Ambient temperature 2: 83 percent / N2H4*H2O / methanol / 21.5 h / Heating 3: diethyl ether / 1) 0 deg C, 1 h, 2) rt, 19.5 h 4: 97 percent / 2 M KOH / methanol / 4 h / Ambient temperature 5: 83 percent / Ac2O / tetrahydrofuran / 120 h / Ambient temperature 6: 13 percent / air / various solvent(s) / 2 h / Heating 7: 54 percent / Ph3P / 1.5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 7 p. 2105 - 2114
