6,7,12,13-四氢-5H-吲哚并[2,3-a]吡咯并[3,4-c]咔唑-5-酮合成路线 （共 45 条）
反应条件
1: diethyl ether / 1) 0 deg C, 1 h, 2) rt, 19.5 h 2: 97 percent / 2 M KOH / methanol / 4 h / Ambient temperature 3: 83 percent / Ac2O / tetrahydrofuran / 120 h / Ambient temperature 4: 13 percent / air / various solvent(s) / 2 h / Heating 5: 54 percent / Ph3P / 1.5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 7 p. 2105 - 2114
反应条件
1: 83 percent / N2H4*H2O / methanol / 21.5 h / Heating 2: diethyl ether / 1) 0 deg C, 1 h, 2) rt, 19.5 h 3: 97 percent / 2 M KOH / methanol / 4 h / Ambient temperature 4: 83 percent / Ac2O / tetrahydrofuran / 120 h / Ambient temperature 5: 13 percent / air / various solvent(s) / 2 h / Heating 6: 54 percent / Ph3P / 1.5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 7 p. 2105 - 2114
反应条件
1: 83 percent / Ac2O / tetrahydrofuran / 120 h / Ambient temperature 2: 13 percent / air / various solvent(s) / 2 h / Heating 3: 54 percent / Ph3P / 1.5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 7 p. 2105 - 2114
反应条件
1: 13 percent / air / various solvent(s) / 2 h / Heating 2: 54 percent / Ph3P / 1.5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 7 p. 2105 - 2114
反应条件
1: 97 percent / 2 M KOH / methanol / 4 h / Ambient temperature 2: 83 percent / Ac2O / tetrahydrofuran / 120 h / Ambient temperature 3: 13 percent / air / various solvent(s) / 2 h / Heating 4: 54 percent / Ph3P / 1.5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 7 p. 2105 - 2114
反应条件
1: 99 percent / CeCl3*7H2O, NaBH4 / methanol / 26 h / Ambient temperature 2: 71 percent / Ph3P, diethyl azodicarboxylate / tetrahydrofuran / 26 h / Ambient temperature 3: 83 percent / N2H4*H2O / methanol / 21.5 h / Heating 4: diethyl ether / 1) 0 deg C, 1 h, 2) rt, 19.5 h 5: 97 percent / 2 M KOH / methanol / 4 h / Ambient temperature 6: 83 percent / Ac2O / tetrahydrofuran / 120 h / Ambient temperature 7: 13 percent / air / various solvent(s) / 2 h / Heating 8: 54 percent / Ph3P / 1.5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 7 p. 2105 - 2114
反应条件
in methanol Irradiation;
参考文献
Sarstedt, Burkhard; Winterfeldt, Ekkehard
Heterocycles, 1983 , vol. 20, # 3 p. 469 - 476
反应条件
1: diethyl ether / 0.17 h / Ambient temperature 2: diethyl ether / 1) 0 deg C, 1 h, 2) rt, 19.5 h 3: 97 percent / 2 M KOH / methanol / 4 h / Ambient temperature 4: 83 percent / Ac2O / tetrahydrofuran / 120 h / Ambient temperature 5: 100 percent / various solvent(s) / 1 h 6: air / various solvent(s) / 4 h / Heating 7: 54 percent / Ph3P / 1.5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 7 p. 2105 - 2114
反应条件
1: air / various solvent(s) / 4 h / Heating 2: 54 percent / Ph3P / 1.5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 7 p. 2105 - 2114
反应条件
sodium tetrahydroborate; cobalt(II) chloride in tetrahydrofuran; methanol 1 h; Ambient temperature;
参考文献
Beccalli, Egle M.; Gelmi, Maria Luisa; Marchesini, Alessandro
Tetrahedron, 1998 , vol. 54, # 24 p. 6909 - 6918
