N,N-二乙基-5-氧代-L-脯氨酰胺合成路线 （共 4 条）
反应条件
DMEG; triethylamine in tetrahydrofuran
0 deg C, 15 min. then room temp. 16 h;
参考文献
Okawa, Tomohiro; Sugimori, Toshiyuki; Eguchi, Shoji; Kakehi, Akikazu
Heterocycles, 1998 , vol. 47, # 1 p. 375 - 382
反应条件
in dichloromethane
T=-10 - 0°C; 12 h;
参考文献
Rigo; El Ghammarti; Gautret; Couturier
Synthetic Communications, 1994 , vol. 24, # 18 p. 2597 - 2607
反应条件
1: 100 percent Chromat. / oxalyl chloride / CH2Cl2 / Heating
2: 53 percent / CH2Cl2 / 12 h / -10 - 0 °C
View Scheme
参考文献
Rigo; El Ghammarti; Gautret; Couturier
Synthetic Communications, 1994 , vol. 24, # 18 p. 2597 - 2607
反应条件
1: 100 percent / saccharin / 2.5 h / Heating
2: 100 percent Chromat. / oxalyl chloride / CH2Cl2 / Heating
3: 53 percent / CH2Cl2 / 12 h / -10 - 0 °C
View Scheme
参考文献
Rigo; El Ghammarti; Gautret; Couturier
Synthetic Communications, 1994 , vol. 24, # 18 p. 2597 - 2607
