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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
858218-65-2
合成路线
（共 9 条）
854050-00-3
→
反应条件
858218-65-2
反应条件
sodium dithionite in water
参考文献
Su, Chung-Ren; Shen, Yuh-Chiang; Kuo, Ping-Chung; Leu, Yann-Lii; Damu, Amooru G.; Wang, Yea-Hwey; Wu, Tian-Shung
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 24 p. 6155 - 6160
918549-44-7
→
反应条件
858218-65-2
反应条件
1: 91 percent / BCl3 / CH2Cl2 2: 91 percent / H5IO6; CrO3 / acetonitrile; H2O 3: 83 percent / Na2S2O4 / H2O View Scheme
参考文献
Su, Chung-Ren; Shen, Yuh-Chiang; Kuo, Ping-Chung; Leu, Yann-Lii; Damu, Amooru G.; Wang, Yea-Hwey; Wu, Tian-Shung
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 24 p. 6155 - 6160
75792-35-7
2-异丙氧基-3-甲氧基苯甲醛
→
反应条件
858218-65-2
反应条件
1: m-CPBA / CH2Cl2 2: NaOH / methanol 3: 85 percent / KI; K2CO3 / acetone 4: 91 percent / BCl3 / CH2Cl2 5: 91 percent / H5IO6; CrO3 / acetonitrile; H2O 6: 83 percent / Na2S2O4 / H2O View Scheme
参考文献
Su, Chung-Ren; Shen, Yuh-Chiang; Kuo, Ping-Chung; Leu, Yann-Lii; Damu, Amooru G.; Wang, Yea-Hwey; Wu, Tian-Shung
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 24 p. 6155 - 6160
148-53-8
邻香草醛
→
反应条件
858218-65-2
反应条件
1: 94 percent / K2CO3 / dimethylformamide 2: m-CPBA / CH2Cl2 3: NaOH / methanol 4: 85 percent / KI; K2CO3 / acetone 5: 91 percent / BCl3 / CH2Cl2 6: 91 percent / H5IO6; CrO3 / acetonitrile; H2O 7: 83 percent / Na2S2O4 / H2O View Scheme
参考文献
Su, Chung-Ren; Shen, Yuh-Chiang; Kuo, Ping-Chung; Leu, Yann-Lii; Damu, Amooru G.; Wang, Yea-Hwey; Wu, Tian-Shung
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 24 p. 6155 - 6160
154013-27-1
→
反应条件
858218-65-2
反应条件
1: 91 percent / H5IO6; CrO3 / acetonitrile; H2O 2: 83 percent / Na2S2O4 / H2O View Scheme
参考文献
Su, Chung-Ren; Shen, Yuh-Chiang; Kuo, Ping-Chung; Leu, Yann-Lii; Damu, Amooru G.; Wang, Yea-Hwey; Wu, Tian-Shung
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 24 p. 6155 - 6160
55020-67-2
→
反应条件
858218-65-2
反应条件
1: HNO3; acetic acid 2: zinc-powder; aqueous H2SO4; ethanol View Scheme
参考文献
King et al.
Journal of the Chemical Society, 1954 , p. 4594,4599
100-44-7
苄基氯
→
反应条件
858218-65-2
反应条件
1: K2CO3; acetone 2: HNO3; acetic acid 3: zinc-powder; aqueous H2SO4; ethanol View Scheme
参考文献
King et al.
Journal of the Chemical Society, 1954 , p. 4594,4599
488-17-5
3-甲基苯邻二酚
→
反应条件
858218-65-2
反应条件
1: K2CO3; acetone 2: HNO3; acetic acid 3: zinc-powder; aqueous H2SO4; ethanol View Scheme
参考文献
King et al.
Journal of the Chemical Society, 1954 , p. 4594,4599
858218-65-2
+
77-78-1
硫酸二甲酯
→
反应条件
855242-15-8
反应条件
sodium hydroxide in water
参考文献
Su, Chung-Ren; Shen, Yuh-Chiang; Kuo, Ping-Chung; Leu, Yann-Lii; Damu, Amooru G.; Wang, Yea-Hwey; Wu, Tian-Shung
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 24 p. 6155 - 6160
