N-BOC-1,2,3,6-四氢吡啶合成路线 （共 32 条）
反应条件
tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butylate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in 1,4-dioxane T=110°C; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 14, # 16 p. 4792 - 4795
反应条件
1: sodium hydrogencarbonate / ethanol; water / 4.5 h / 20 °C 2: 4-(N,N-dimethlyamino)pyridine / dichloromethane / 2 h / 0 °C 3: caesium carbonate / dimethyl sulfoxide / 3 h / 120 °C View Scheme
参考文献
Tetrahedron, , vol. 67, # 7 p. 1485 - 1500
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in deuterated toluene T=29.84°C; Reagent/catalyst;
参考文献
Chemistry - A European Journal, , vol. 19, # 48 p. 16403 - 16414
反应条件
sodium hydride in N,N-dimethyl-formamide T=0 - 120°C; Title compound not separated from byproducts.;
参考文献
Synthetic Communications, , vol. 38, # 4 p. 517 - 524
反应条件
sodium hydride in N,N-dimethyl-formamide T=120°C; Title compound not separated from byproducts.;
参考文献
Synthetic Communications, , vol. 38, # 4 p. 517 - 524
反应条件
sodium hydride in N,N-dimethyl-formamide T=0 - 120°C; Title compound not separated from byproducts.;
参考文献
Synthetic Communications, , vol. 38, # 4 p. 517 - 524
反应条件
sodium hydride in N,N-dimethyl-formamide T=120°C; Title compound not separated from byproducts.;
参考文献
Synthetic Communications, , vol. 38, # 4 p. 517 - 524
反应条件
1: 93 percent / benzene / 1 h / Heating 2: NH2NH2*H2O; KOH / ethane-1,2-diol / 1.5 h / Heating 3: CHCl3 / 12 h / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 17, # 16 p. 4523 - 4526
反应条件
1: NH2NH2*H2O; KOH / ethane-1,2-diol / 1.5 h / Heating 2: CHCl3 / 12 h / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 17, # 16 p. 4523 - 4526
反应条件
1: NaBH4 / ethanol / 6 h / 20 °C 2: 93 percent / benzene / 1 h / Heating 3: NH2NH2*H2O; KOH / ethane-1,2-diol / 1.5 h / Heating 4: CHCl3 / 12 h / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 17, # 16 p. 4523 - 4526
