5-氟-3-碘-1H-吲唑合成路线 （共 3 条）
反应条件
iodine; potassium hydroxide in N,N-dimethyl-formamide T=20°C; 1 h;
参考文献
Synthesis, , # 19 art. no. T48411SS, p. 3089 - 3098
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; triethylamine in toluene T=80°C; P=750.075 Torr; Autoclave;
参考文献
Buchstaller, Hans-Peter; Wilkinson, Kai; Burek, Kasimir; Nisar, Yasmin
Synthesis, 2011 , # 19 art. no. T48411SS, p. 3089 - 3098
反应条件
1: 4-(N,N-dimethlyamino)pyridine; triethylamine / 20 °C
2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / 1,4-dioxane; water / 1 h / 120 °C / |Microwave irradiation
View Scheme
参考文献
Youngsaye, Willmen; Hartland, Cathy L.; Morgan, Barbara J.; Ting, Amal; Nag, Partha P.; Vincent, Benjamin; Mosher, Carrie A.; Bittker, Joshua A.; Dandapani, Sivaraman; Palmer, Michelle; Whitesell, Luke; Lindquist, Susan; Schreiber, Stuart L.; Munoz, Benito
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1501 - 1507
