1-(3,7-二甲基-6-辛烯-1-基)-5-苯基-1H-咪唑合成路线 (共 7 条)
反应条件
sodium hydride in N,N-dimethyl-formamide
1.) r.t., 1 h, 2.) r.t., 15 h;
参考文献
Kuwano, Eiichi; Takeya, Ryuko; Eto, Morifusa
Agricultural and Biological Chemistry, 1984 , vol. 48, # 12 p. 3115 - 3120
反应条件
sodium hydride in N,N-dimethyl-formamide
参考文献
Kuwano; Takeya; Eto
Agricultural and Biological Chemistry, 1983 , vol. 47, # 4 p. 921 - 923
反应条件
1: phosphorus oxychloride, triethylamine / 1,2-dimethoxy-ethane / 1 h / 0 °C
2: methanol / Ambient temperature
View Scheme
参考文献
Kikuchi, Masamichi; Kuwano, Eiichi; Nakashima, Yukiko; Eto, Morifusa
Bioscience, Biotechnology, and Biochemistry, 1992 , vol. 56, # 1 p. 161 - 162
反应条件
1: potassium tert-butoxide / 1,2-dimethoxy-ethane
2: phosphorus oxychloride, triethylamine / 1,2-dimethoxy-ethane / 1 h / 0 °C
3: methanol / Ambient temperature
View Scheme
参考文献
Kikuchi, Masamichi; Kuwano, Eiichi; Nakashima, Yukiko; Eto, Morifusa
Bioscience, Biotechnology, and Biochemistry, 1992 , vol. 56, # 1 p. 161 - 162
反应条件
1: MgSO4 / CH2Cl2 / 3 h / Heating
2: K2CO3 / methanol / 2 h / Heating
View Scheme
参考文献
Kuwano, Eiichi; Takeya, Ryuko; Eto, Morifusa
Agricultural and Biological Chemistry, 1984 , vol. 48, # 12 p. 3115 - 3120
反应条件
potassium carbonate in methanol
2 h; Heating; Yield given;
参考文献
Kuwano, Eiichi; Takeya, Ryuko; Eto, Morifusa
Agricultural and Biological Chemistry, 1984 , vol. 48, # 12 p. 3115 - 3120
反应条件
in methanol
Ambient temperature;
参考文献
Kikuchi, Masamichi; Kuwano, Eiichi; Nakashima, Yukiko; Eto, Morifusa
Bioscience, Biotechnology, and Biochemistry, 1992 , vol. 56, # 1 p. 161 - 162