5-(1-羟基乙亚基)-2,2-二甲基-1,3-二氧杂环己-4,6-二酮合成路线 （共 21 条）
参考文献
Giacomelli, Giampaolo; Porcheddu, Andrea; Salaris, Margherita; Taddei, Maurizio
European Journal of Organic Chemistry, 2003 , # 3 p. 537 - 541
参考文献
Roh, Eun Joo; Keller, Jason M.; Olah, Zoltan; Iadarola, Michael J.; Jacobson, Kenneth A.
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 20 p. 9349 - 9358
反应条件
in toluene 1 h; Heating;
参考文献
Giacomelli, Giampaolo; Porcheddu, Andrea; Salaris, Margherita; Taddei, Maurizio
European Journal of Organic Chemistry, 2003 , # 3 p. 537 - 541
反应条件
T=70°C; Ring cleavage; Decarboxylation; 6 h;
参考文献
Bhandari, Ashok; Li, Bei; Gallop, Mark A.
Synthesis, 1999 , # 11 p. 1951 - 1960
反应条件
in tetrahydrofuran 4 h; Heating;
参考文献
Lermer, Leonard; Neeland, Edward G.; Ounsworth, James P.; Sims, Russell J.; Tischler, Samuel A.; Weiler, Larry
Canadian Journal of Chemistry, 1992 , vol. 70, # 5 p. 1427 - 1445
反应条件
Yield given. Multistep reaction;
参考文献
Tietze, Lutz F.; Steinmetz, Adrian; Balkenhohl, Friedhelm
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 10 p. 1303 - 1306
反应条件
T=70°C; Ring cleavage; Decarboxylation; 6 h;
参考文献
Bhandari, Ashok; Li, Bei; Gallop, Mark A.
Synthesis, 1999 , # 11 p. 1951 - 1960
反应条件
in toluene Esterification; 4 h; Heating;
参考文献
Fleming, Ian; Ramarao, Chandrashekar
Chemical Communications, 1999 , # 12 p. 1113 - 1114
反应条件
pyridine in dichloromethane
T=0 - 20°C; Acylation;
参考文献
Sorensen, Ulrik S.; Falch, Erik; Krogsgaard-Larsen, Povl
Journal of Organic Chemistry, 2000 , vol. 65, # 4 p. 1003 - 1007
反应条件
1: in dichloromethane
120 h; Heating;
2: With water in tetrahydrofuran
T=20°C; 4 h;
参考文献
Akue-Gedu, Rufine; El-Hafidi, Hayate; Rigo, Benoit; Couturier, Daniel
Journal of Heterocyclic Chemistry, 2006 , vol. 43, # 2 p. 365 - 369
