1: diazomethyl-trimethyl-silane With lithium diisopropyl amide in various solvents
T=-78°C; 1 h;
2: 3-bromo-4-methoxy benzaldehyde in various solvents
T=-78 - 20°C; 3 h; Further stages.;
参考文献
Odlo, Kristin; Fournier-Dit-Chabert, Jeremie; Ducki, Sylvie; Gani, Osman A.B.S.M.; Sylte, Ingebrigt; Hansen, Trond Vidar
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 18 p. 6874 - 6885
