反应条件
1: tert-butyllithium / 1.) THF, pentane, room temperature, 2.) 1 h
2: 1.) ozone, 2.) dimethyl sulfide / 1.) ethyl acetate, -78 deg C, 2.) room temperature, 5 h
3: 81 percent / benzene / 4 h / 65 °C
View Scheme
参考文献
Card,P.J.; Friedli,F.E.; Shechter,H.
Journal of the American Chemical Society, 1983 , vol. 105, p. 6104