1: in N,N-dimethyl-formamide
6 h; Inert atmosphereReflux;
2: With hydrogenchloride in dichloromethane; water
T=20°C; 0.166667 h; Inert atmosphere;
参考文献
Hyun, Min Young; Jo, Young Dan; Lee, Jun Ho; Lee, Hong Gyu; Park, Hyun Min; Hwang, In Hong; Kim, Kyeong Beom; Lee, Suk Joong; Kim, Cheal
Chemistry - A European Journal, 2013 , vol. 19, # 5 p. 1810 - 1818
in dimethylformamide
MnCl2*4HO was added to porphyrin followed by reflux for 24 h in DMF, washed with HCl; in accordance to Rachford, A. A.; Petersen, J. L.; Rack, J. J. Inorg. Chem. 2005, 44, 8065-8075;
参考文献
Fukuzumi, Shunichi; Fujioka, Naofumi; Kotani, Hiroaki; Ohkubo, Kei; Lee, Yong-Min; Nam, Wonwoo
Journal of the American Chemical Society, 2009 , vol. 131, # 47 p. 17127 - 17134
