5-叔丁基-2-甲氧基苯甲醛合成路线 (共 10 条)
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C; 20 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 131, # 32 p. 11509 - 11518
反应条件
n-butyllithium 1.) ether, hexane, 20 h, 2.) 30 min; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 112, # 13 p. 5212 - 5219
反应条件
trifluoroacetic acid 24 h; Heating;
参考文献
Synthesis, , # 7 p. 1029 - 1032
反应条件
1: aqueous HCl 2: water View Scheme
参考文献
Journal of Organic Chemistry, , vol. 16, p. 586,606
参考文献
Journal of Organic Chemistry, , vol. 16, p. 586,606
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 43, # 4 p. 857 - 863
参考文献
American Chemical Journal, , vol. 16, p. 635
参考文献
Prescott,B.; Li,C.P.
Journal of Medicinal Chemistry, 1964 , vol. 7, p. 383 - 385
反应条件
1: 1.) Mg / 1.) THF, reflux, 12 h, 2.) THF, reflux, 12 h
2: 90 percent / AlH2Cl / diethyl ether / 17 h / Heating
View Scheme
参考文献
Yamato, Takehiko; Inoue, Hisataka; Maeda, Kenji; Tashiro, Masashi
Journal of Chemical Research, Miniprint, 1996 , # 7 p. 1731 - 1745
反应条件
nitric acid; acetic anhydride; acetic acid
参考文献
Carpenter et al.
Journal of Organic Chemistry, 1951 , vol. 16, p. 586,606