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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-甲氧基联苯
合成路线
（共 216 条）
90-04-0
邻甲氧基苯胺
+
98-80-6
苯硼酸
→
反应条件
86-26-0
2-甲氧基联苯
反应条件
1: 2-methoxy-phenylamine With tert.-butylnitrite; boron trifluoride diethyl etherate in tetrahydrofuran T=0°C; 0.5 h; 2: 3,4,5-trimethoxyphenylboronic acid With SIDip*HCl; palladium diacetate in tetrahydrofuran T=20°C; Suzuki-Miyaura coupling; 4 h; Further stages.;
参考文献
Andrus; Song
Organic letters, 2001 , vol. 3, # 23 p. 3761 - 3764
766-51-8
2-氯苯甲醚
+
24388-23-6
苯硼酸频哪醇酯
→
反应条件
86-26-0
2-甲氧基联苯
反应条件
potassium fluoride; 18-crown-6 ether; bis-phenanthrylimidazolium chloride; palladium diacetate in tetrahydrofuran; water T=50°C; Suzuki-Miyaura coupling; 10 h;
参考文献
Song, Chun; Ma, Yudao; Chai, Qiang; Ma, Chanqin; Jiang, Wei; Andrus, Merritt B.
Tetrahedron, 2005 , vol. 61, # 31 p. 7438 - 7446
59099-58-0
+
98-80-6
苯硼酸
→
反应条件
86-26-0
2-甲氧基联苯
反应条件
potassium fluoride; 18-crown-6 ether; bis-phenanthrylimidazolium chloride; palladium diacetate in tetrahydrofuran T=20°C; Suzuki-Miyaura coupling; 3 h;
参考文献
Song, Chun; Ma, Yudao; Chai, Qiang; Ma, Chanqin; Jiang, Wei; Andrus, Merritt B.
Tetrahedron, 2005 , vol. 61, # 31 p. 7438 - 7446
529-28-2
2-碘苯甲醚
→
反应条件
86-26-0
2-甲氧基联苯
反应条件
N-ethyl-N,N-diisopropylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in water; isopropyl alcohol T=100°C; Suzuki coupling; 0.166667 h; microwave irradiation;
参考文献
Kabalka, George W.; Al-Masum, Mohammad
Tetrahedron Letters, 2005 , vol. 46, # 37 p. 6329 - 6331
578-57-4
2-溴苯甲醚
+
2996-92-1
苯基三甲氧基硅烷
→
反应条件
86-26-0
2-甲氧基联苯
反应条件
sodium hydroxide; Na2[PdCl4]; sodium lauryl sulfate T=100°C; Hiyama cross-coupling; 0.0833333 h;
参考文献
Ranu, Brindaban C.; Dey, Raju; Chattopadhyay, Kalicharan
Tetrahedron Letters, 2008 , vol. 49, # 21 p. 3430 - 3432
→
反应条件
86-26-0
2-甲氧基联苯
反应条件
palladium diacetate; tri-cyclo-hexyl-phosphine in ethylene glycol dimethyl ether T=20°C; 3 h;
参考文献
Ku, Shih-Lun; Hui, Xin-Ping; Chen, Chien-An; Kuo, Yi-Ying; Gau, Han-Mou
Chemical Communications, 2007 , # 37 p. 3847 - 3849
529-28-2
2-碘苯甲醚
+
143-66-8
四苯硼钠
→
反应条件
86-26-0
2-甲氧基联苯
反应条件
1: sodium tetraphenyl borate With Amberlite(R)IRA-900 resin in water 2: 1-iodo-2-methoxybenzene With palladium diacetate in N,N-dimethyl-formamide T=90°C; Suzuki-Miyaura coupling reaction; 4 h; Further stages.;
参考文献
Basu, Basudeb; Das, Sajal; Kundu, Sekhar; Mandal, Bablee
Synlett, 2008 , # 2 p. 255 - 259
108-86-1
溴代苯
+
529-28-2
2-碘苯甲醚
→
反应条件
92-52-4
联苯
+
86-26-0
2-甲氧基联苯
+
100-66-3
苯甲醚
反应条件
1: bromobenzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; Negishi coupling reaction; 0.166667 h; Inert atmosphere; 2: With zinc(II) chloride in tetrahydrofuran; hexane T=-78 - 20°C; Negishi coupling reaction; Inert atmosphere; 3: 1-iodo-2-methoxybenzene With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran; hexane T=60°C; Negishi coupling reaction; 2 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 131, # 29 p. 10201 - 10210
766-51-8
2-氯苯甲醚
+
780-69-8
苯基三乙氧基硅烷
→
反应条件
86-26-0
2-甲氧基联苯
反应条件
Pd((CH3)2C6H3NC(CH3)CHC(CH3)NC6H3(CH3)2)(CH3)(P(CH2CH3)3); tetrabutylammomium bromide; sodium hydroxide in water T=60°C; Hiyama coupling; 8 h; Inert atmosphere;
参考文献
Lee, Dong-Hwan; Jung, Ji-Young; Jin, Myung-Jong
Chemical Communications, 2010 , vol. 46, # 47 p. 9046 - 9048
462-06-6
氟苯
+
16750-63-3
2-甲氧基苯基溴化镁
→
反应条件
86-26-0
2-甲氧基联苯
反应条件
C37H30OP2; ZnCl2*TMEDA; Ni(acac)2 in tetrahydrofuran T=0 - 70°C; 13 h; Inert atmosphere;
参考文献
Nakamura, Yuki; Yoshikai, Naohiko; Ilies, Laurean; Nakamura, Eiichi
Organic Letters, 2012 , vol. 14, # 13 p. 3316 - 3319
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