暂无反应条件数据

sodium hydroxide T=100°C; 2 h;

1: phenol / 110 °C 2: thionyl chloride View Scheme

(NH4)2CO3; phenol T=120°C; Substitution; 0.75 h;

potassium hydroxide; hydrogen; oxygen; iron(II) chloride; nickel 1.) r.t., benzene, methanol; 2.) 60 deg C, 4 h; Yield given. Multistep reaction;

暂无反应条件数据

暂无反应条件数据

phenol T=100°C;

phenol

1: 1.) hydrogen, potassium hydroxide; 2.) ferrous chloride, oxygen / 1.) Raney-nickel / 1.) r.t., benzene, methanol; 2.) 60 deg C, 4 h 2: 96 percent / KNO3 / aq. H2SO4 / 1 h / -2 - 0 °C 3: 1.) aluminium amalgame; 2.) oxygen / 1.) ethanol, 95 deg C, 1 h; 2.) 8 h 4: 1.) sodium nitrite, p-sulfanilic acid, sodium acetate; 3.) sodium dithionite, 2.5 percent sodium hydroxide / 1.) acetic acid, -2 deg C, 1 h; 2.) 33 percent aq. acetic acid, 0 deg C, 15 min; 3.) 1 h 5: 1.5 M sulfuric acid, potassium dichromate / CHCl3 6: 66 percent / bromine / CHCl3 / 24 h / Ambient temperature View Scheme