2,3-二甲氧基苯甲醛合成路线 （共 174 条）
反应条件
sodium hydroxide; potassium permanganate 1.) 50 deg C, 1 h; 2.) room temp., 12 h.;
参考文献
Stuart; Khora; McKenney Jr.; Castle
Journal of Heterocyclic Chemistry, 1987 , vol. 24, # 6 p. 1589 - 1594
参考文献
Perkin; Robinson
Journal of the Chemical Society, 1914 , vol. 105, p. 2384
参考文献
Perkin; Stoyle
Journal of the Chemical Society, 1923 , vol. 123, p. 3174
反应条件
1.1: 85 percent / 1 h / 110 °C 2.1: 85 percent / NaBH4 / methanol / 2 h / Heating 3.1: HOAc; CuSO4; NaCl / 0.5 h / 50 °C 3.2: 60 percent / AcOH / 6 h / 85 °C View Scheme
参考文献
Bian, Xiaoli; He, Langchong; Yang, Guangde
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 5 p. 1380 - 1383
反应条件
dihydrogen peroxide; sulfuric acid in methanol 63 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 49, # 24 p. 4740 - 4741
反应条件
1: Ag2O; aqueous NaOH 2: concentrated H2SO4; 1,2-dichloro-ethane View Scheme
参考文献
McChesney; Kabra; Fraher
Journal of Pharmaceutical Sciences, 1979 , vol. 68, # 9 p. 1116 - 1120
反应条件
boron tribromide in dichloromethane 24 h; Ambient temperature;
参考文献
Oppolzer; Robbiani
Helvetica Chimica Acta, 1983 , vol. 66, # 4 p. 1119 - 1128
反应条件
1: 85 percent / benzoic acid, piperidine / benzene / Heating 2: Mg, copper iodide / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Katakawa, Jun'Ichi; Yoshimatsu, Hideaki; Yoshida, Morihiro; Zhang, Yong; Irie, Hiroshi; Yajima, Haruaki
Chemical & Pharmaceutical Bulletin, 1988 , vol. 36, # 10 p. 3928 - 3932
反应条件
1: NaH, Me2SO / tetrahydrofuran / 5 h / 5 °C
2: 57.6 g / H2 / 5percent Pd/C / acetic acid
3: PCl4, SnCl4
View Scheme
参考文献
Bonner, Lisa A.; Laban, Uros; Chemel, Benjamin R.; Juncosa, Jose I.; Lill, Markus A.; Watts, Val J.; Nichols, David E.
ChemMedChem, 2011 , vol. 6, # 6 p. 1024 - 1040
反应条件
1: 49 percent / HNO3 / acetic acid / 0.75 h / Ambient temperature
2: 95 percent / boron tribromide / CH2Cl2 / Ambient temperature
View Scheme
参考文献
Fukuyama, Yoshiyasu; Iwatsuki, Chie; Kodama, Mitsuaki; Ochi, Masamitsu; Kataoka, Kumi; Shibata, Kozo
Tetrahedron, 1998 , vol. 54, # 34 p. 10007 - 10016
