2,3-二甲氧基苯甲醛合成路线 （共 174 条）
反应条件
piperidine in pyridine Heating;
参考文献
Jardon, Phillip W.; Vickery, Euin H.; Pahler, Leon F.; Pourahmady, Naser; Mains, Gilbert J.; Eisenbraun, Edmund J.
Journal of Organic Chemistry, 1984 , vol. 49, # 12 p. 2130 - 2135
反应条件
ammonium acetate in butan-1-ol Rodionov reaction; Heating;
参考文献
Russian Journal of General Chemistry, , vol. 75, # 7 p. 1113 - 1124
反应条件
1: permanganate 2: hydrogen iodide / 100 °C 3: aqueous-alcoholic KOH-solution; hydrogen stream 4: thionyl chloride View Scheme
参考文献
Perkin; Trikojus
Journal of the Chemical Society, 1926 , p. 2932
反应条件
1: With palladium 10 on activated carbon; hydrogen in ethyl acetate T=20°C; P=258.581 Torr; 15 h; Large scale; 2: With 1,3-dibromo-5,5-dimethyl-hydantoin in ethyl acetate T=15°C; 12 h; Large scale;
参考文献
Connolly, Terrence J.; Matchett, Michael; McGarry, Patrick; Sukhtankar, Sunil; Zhu, Jiang
Organic Process Research and Development, 2004 , vol. 8, # 4 p. 624 - 627
反应条件
1: alcoholic KOH-solution / 20 °C 2: diethyl ether; HCl 3: benzene / 100 - 120 °C View Scheme
参考文献
Cao, Weidi; Liu, Xiaohua; Wang, Wentao; Lin, Lili; Feng, Xiaoming
Organic Letters, 2011 , vol. 13, # 4 p. 600 - 603
反应条件
ethanol beim anschliessenden Hydrieren an Raney-Nickel;
参考文献
Venkov, Atanas P.; Vodenicharov, Daniel M.
Synthesis, 1990 , # 3 p. 253 - 255
反应条件
1.1: palladium 10 on activated carbon; hydrogen / ethyl acetate / 15 h / 20 °C / 258.58 Torr / |Large scale 1.2: 12 h / 15 °C / |Large scale 2.1: magnesium; methyl-magnesium chloride / tetrahydrofuran / 25 °C / |Inert atmosphere; |Large scale 2.2: -60 °C / |Inert atmosphere; |Large scale 2.3: 1 h / 25 - 30 °C / |Inert atmosphere; |Large scale View Scheme
参考文献
Connolly, Terrence J.; Matchett, Michael; McGarry, Patrick; Sukhtankar, Sunil; Zhu, Jiang
Organic Process Research and Development, 2004 , vol. 8, # 4 p. 624 - 627
反应条件
piperidine; pyridine
参考文献
Chang, Sheng; Yin, Shi-Liang; Wang, Jian; Jing, Yong-Kui; Dong, Jin-Hua
Molecules, 2009 , vol. 14, # 10 p. 4166 - 4179
反应条件
sodium acetate T=200°C;
参考文献
v. Krannichfeldt
Chemische Berichte, 1913 , vol. 46, p. 4024
参考文献
Perkin; Stoyle
Journal of the Chemical Society, 1923 , vol. 123, p. 3174
