1: dibenzopyrrole With potassium hydroxide in N,N-dimethyl-formamide T=20°C; 1 h; 2: (R/S)-2-Bromomethyl-oxirane in N,N-dimethyl-formamide T=20°C; 20 h; Cooling with ice;
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Patent: US2013/303524 A1, 2013 ;
Location in patent: Paragraph 0254-0255 ;
1: 1H-imidazole; dibenzopyrrole With lithium tert-butylate in acetonitrile; tert-butyl alcohol T=20°C; 0.05 h; Glovebox; 2: iodobenzene With copper(l) iodide in acetonitrile; tert-butyl alcohol T=20°C; 2 h; Irradiation;
参考文献
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Journal of the American Chemical Society, 2013 , vol. 135, # 35 p. 13107 - 13112
E. coli (pHA171); isoropyl β-D-thiogalactopyranoside; 6-[D(-)-α-aminophenylacetamido]penicillanic acid; D-glucose; thiamine hydrochloride in various solvent(s) T=30°C;
参考文献
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