3,4,5-三甲氧基苯甲醛合成路线 （共 427 条）
反应条件
piperidine; sulfuric acid 1) pyridine; Yield given. Multistep reaction;
参考文献
European Journal of Medicinal Chemistry, , vol. 23, # 1 p. 53 - 62
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 35, # 6 p. 419 - 428
反应条件
in methanol Ambient temperature;
参考文献
Manchand, Percy S.; Rosen, Perry; Belica, Peter S.; Oliva, Gloria V.; Perrotta, Agostino V.; Wong, Harry S.
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3531 - 3535
反应条件
hydrogen; platinum on activated charcoal in methanol; water
参考文献
Elslager, Edward F.; Johnson, Judith L.; Werbel, Leslie M.
Journal of Medicinal Chemistry, 1981 , vol. 24, # 2 p. 140 - 145
反应条件
1: With anhydrous butyl ether; bis[3,5-bis(trifluoromethyl)diphenyl] diselenide in 2,2,2-trifluoroethanol T=20°C; Baeyer-Villiger oxidation; 0.25 h; 2: With potassium hydroxide in methanol 2 h; Further stages.;
参考文献
Ten Brink; Vis; Arends; Sheldon
Journal of Organic Chemistry, 2001 , vol. 66, # 7 p. 2429 - 2433
反应条件
anhydrous butyl ether; bis[3,5-bis(trifluoromethyl)diphenyl] diselenide in 2,2,2-trifluoroethanol T=20°C; Baeyer-Villiger oxidation; 0.25 h;
参考文献
Ten Brink; Vis; Arends; Sheldon
Journal of Organic Chemistry, 2001 , vol. 66, # 7 p. 2429 - 2433
反应条件
sodium hypochlorite; phosphate buffer; hypochlorous acid in water T=25°C; Chlorination; 24 h; Title compound not separated from byproducts;
参考文献
Langvik, Vivi-Ann; Hormi, Osmo
Chemosphere, 1994 , vol. 28, # 6 p. 1111 - 1118
反应条件
sodium hypochlorite; sodium chlorite in water Chlorination; pH=2; 48 h; Formation of xenobiotics;
参考文献
Huixian, Zou; Junhe, Lu; Zhuo, Chen; Chengyong, Yang; Jinqi, Zhang; Wen, Zhou
Water Research, 2000 , vol. 34, # 1 p. 225 - 229
参考文献
Sharp
Journal of the Chemical Society, 1936 , p. 1234
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in methanol T=20°C; P=760.051 Torr; 1.5 h;
参考文献
Xing, Lixin; Wang, Xinyan; Cheng, Chuanjie; Zhu, Rui; Liu, Bo; Hu, Yuefei
Tetrahedron, 2007 , vol. 63, # 38 p. 9382 - 9386
