3,4,5-三甲氧基苯甲醛合成路线 (共 427 条)
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; P=760.051 Torr; 2 h;
参考文献
Tetrahedron, , vol. 63, # 38 p. 9382 - 9386
反应条件
hydrogen; acetic acid; palladium on activated charcoal in methanol T=20°C; P=760.051 Torr; 2 h;
参考文献
Tetrahedron, , vol. 63, # 38 p. 9382 - 9386
反应条件
chloroform; 10 Pd/C; hydrogen in methanol T=20°C; P=760.051 Torr; 2 h; chemoselective reaction;
参考文献
Tetrahedron, , vol. 64, # 51 p. 11783 - 11788
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal T=20°C; P=760.051 Torr; 7 h;
参考文献
Tetrahedron, , vol. 63, # 38 p. 9382 - 9386
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal T=20°C; P=760.051 Torr; 0.0833333 h;
参考文献
Tetrahedron, , vol. 63, # 38 p. 9382 - 9386
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal T=20°C; P=760.051 Torr; 0.133333 h;
参考文献
Tetrahedron, , vol. 63, # 38 p. 9382 - 9386
反应条件
1: 83 percent / NH4Cl / methanol / 3 h / Heating 2: 90 percent / 1) Na, 2) H2O, 3) 1N HCl / tetrahydrofuran / 53 h / Ambient temperature View Scheme
参考文献
Azzena, Ugo; Cossu, Sergio; Denurra, Teresa; Melloni, Giovanni; Piroddi, Anna Maria
Synthesis, 1990 , p. 313 - 314
反应条件
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / Inert atmosphere 2: water; potassium hydroxide / tetrahydrofuran / Inert atmosphere 3: potassium carbonate / acetone / Inert atmosphere View Scheme
参考文献
Caldwell, Stuart T.; McPhail, Donald B.; Duthie, Garry G.; Hartley, Richard C.
Canadian Journal of Chemistry, 2012 , vol. 90, # 1 p. 23 - 33
反应条件
palladium diacetate in cyclohexane T=140°C; 24 h; Molecular sieveair;
参考文献
Modak, Atanu; Deb, Arghya; Patra, Tuhin; Rana, Sujoy; Maity, Soham; Maiti, Debabrata
Chemical Communications, 2012 , vol. 48, # 35 p. 4253 - 4255
反应条件
1: 65 percent / piperidine / H2O / 20 h / Heating 2: pyridine View Scheme
参考文献
Rizzacasa, Mark A.; Sargent, Melvyn V.
Australian Journal of Chemistry, 1987 , vol. 40, # 10 p. 1737 - 1743