3,4,5-三甲氧基苯甲醛合成路线 (共 427 条)
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal T=20°C; P=760.051 Torr; 0.0833333 h;
参考文献
Tetrahedron, , vol. 63, # 38 p. 9382 - 9386
反应条件
hydrogenchloride 0.5 h;
参考文献
Xing, Lixin; Wang, Xinyan; Cheng, Chuanjie; Zhu, Rui; Liu, Bo; Hu, Yuefei
Tetrahedron, 2007 , vol. 63, # 38 p. 9382 - 9386
反应条件
aluminum oxide; carbon dioxide; Isopulegol T=200°C; P=110207 Torr; Supercritical conditions;
参考文献
Russian Journal of Physical Chemistry A, , vol. 87, # 3 p. 382 - 387
Kinet. Katal., , vol. 87, # 3 p. 403 - 408,6
反应条件
sodium methylate in methanol T=0°C; 5 h;
参考文献
Boger; Ishizaki; Zarrinmayeh
Journal of Organic Chemistry, 1990 , vol. 55, # 15 p. 4499 - 4502
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Boger; Ishizaki; Zarrinmayeh; Munk; Kitos; Suntornwat
Journal of the American Chemical Society, 1990 , vol. 112, # 24 p. 8961 - 8971
反应条件
in methanol 8.5 h; cooling;
参考文献
Condie, Glenn C.; Channon, Michelle F.; Ivory, Andrew J.; Kumar, Naresh; Black, David StC.
Tetrahedron, 2005 , vol. 61, # 21 p. 4989 - 5004
反应条件
3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; triethylamine in 1,4-dioxane; ethanol Stetter reaction; 30 h; Heating;
参考文献
Bernardes, Lilian Sibelle Campos; Kato, Massuo Jorge; Albuquerque, Sergio; Carvalho, Ivone
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 21 p. 7075 - 7082
反应条件
hydrogenchloride; palladium on activated charcoal 1 h;
参考文献
Xing, Lixin; Wang, Xinyan; Cheng, Chuanjie; Zhu, Rui; Liu, Bo; Hu, Yuefei
Tetrahedron, 2007 , vol. 63, # 38 p. 9382 - 9386
反应条件
2: 1.) BCl3, 2.) HCl / 1.) CH2Cl2, 2.) MeOH 3: Fe(ClO4)3, trifluoroacetic acid / CH2Cl2 4: K2CO3 / dimethylformamide 5: DIBAH / tetrahydrofuran / 0 °C 6: 92 percent 7: 1.) HCO2NH4, PdCl2(PPh3)2, 2.) NaOH 9: 99 percent / LiAlH4 View Scheme
参考文献
Tanaka; Mukaiyama; Mitsuhashi; Wakamatsu
Tetrahedron Letters, 1992 , vol. 33, # 29 p. 4165 - 4168
反应条件
sulfated titania in water T=80°C; 0.2 h;
参考文献
Karmakar, Bikash; Nayak, Anupam; Banerji, Julie
Tetrahedron Letters, 2012 , vol. 53, # 33 p. 4343 - 4346
反应条件
1: pyridine; piperidine 2: thionyl chloride; N,N-dimethylformamide / 1,2-dichloro-ethane / 6 h / Heating View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 37, # 12 p. 961 - 972