3,4,5-三甲氧基苯甲醛合成路线 （共 427 条）
反应条件
hydrogenchloride; water in diethyl ether; toluene T=20°C; 2 h; Inert atmosphere;
参考文献
Perez, Juana M.; Cano, Rafael; Yus, Miguel; Ramon, Diego J.
European Journal of Organic Chemistry, 2012 , # 24 p. 4548 - 4554
反应条件
oxygen; anhydrous cobalt diacetate; Manganese (II) acetate in acetic acid T=110°C; P=2280 Torr; 2 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, # 3 p. 1035 - 1038
反应条件
caesium carbonate in ethylene glycol dimethyl ether T=145°C; 0.416667 h; Microwave irradiationInert atmosphereSealed vessel;
参考文献
Maras, Nenad; Polanc, Slovenko; Kocevar, Marijan
Tetrahedron, 2008 , vol. 64, # 51 p. 11618 - 11624
反应条件
molecular sieve; pyridinium chlorochromate in dichloromethane T=20°C; 8 h;
参考文献
Fernandes, Rodney A.; Kumar, Pradeep
Tetrahedron Letters, 2003 , vol. 44, # 6 p. 1275 - 1278
反应条件
Candida antarctica Lipase A; sodium hydroxide in toluene pH=7; 22.5 h; aq. phosphate bufferEnzymatic reaction;
参考文献
Tetrahedron Asymmetry, , vol. 22, # 24 p. 2144 - 2150
反应条件
Schwartz's reagent in tetrahydrofuran T=20°C; 0.5 h;
参考文献
Leighty, Matthew W.; Spletstoser, Jared T.; Georg, Gunda I.
Organic Syntheses, 2012 , vol. 88, p. 427 - 437
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in tetrahydrofuran; dimethyl sulfoxide 0.416667 h; Ambient temperature;
参考文献
Bose; Venkat Narsaiah; Ravinder Goud
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 8 p. 719 - 721
反应条件
sodium periodate in dichloromethane T=40 - 50°C; Ionic liquid;
参考文献
Hullio, Ahmed Ali; Mastoi; Khan, Khalid
Asian Journal of Chemistry, 2011 , vol. 23, # 12 p. 5411 - 5418
反应条件
dichloro(cycloocta-1,5-diene)palladium(II); N,N-dicyclohexylmethylamine; potassium formiate; tetra-(n-butyl)ammonium iodide; PCy3∙HBF4; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4 in acetonitrile T=80°C; 18 h; Sealed tubeGloveboxInert atmosphere;
参考文献
Korsager, Signe; Taaning, Rolf H.; Lindhardt, Anders T.; Skrydstrup, Troels
Journal of Organic Chemistry, 2013 , vol. 78, # 12 p. 6112 - 6120
反应条件
copper dichloride in N,N-dimethyl-formamide T=120°C;
参考文献
Puri, S. C.; Anand, S. M.; Atal, C. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 294 - 295
