3,4,5-三甲氧基苯甲醛合成路线 （共 427 条）
参考文献
Sharp
Journal of the Chemical Society, 1937 , p. 852
反应条件
1: NaBH4 / methanol / 20 °C 2: SOCl2 / dioxane / 20 °C 3: acetonitrile / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 11, # 16 p. 2205 - 2208
反应条件
water; chloroformic acid ethyl ester; magnesium sulfate Hydrieren des Reaktionsprodukts an Palladium in Benzol;
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 283, p. 190
反应条件
1.1: 84 percent / tetrahydrofuran / -78 - 0 °C 2.1: 91 percent / DMSO; oxalyl chloride; Et3N / CH2Cl2 / -78 °C 3.1: 94 percent / tetrahydrofuran; diethyl ether / -78 °C 4.1: t-BuONO / benzene 4.2: 77 percent / benzene / 0 °C / Photolysis View Scheme
参考文献
Mauthner
Journal fuer Praktische Chemie (Leipzig), 1915 , vol. <2> 92, p. 200
反应条件
diethyl ether; benzene
参考文献
Mauthner
Journal fuer Praktische Chemie (Leipzig), 1910 , vol. <2> 82, p. 279
反应条件
1: acetic anhydride; triethylamine / 140 °C 2: quinoline; copper / 220 °C View Scheme
参考文献
Cao, Xiao-Yan; Yang, Jie; Dai, Fang; Ding, De-Jun; Kang, Yan-Fei; Wang, Fu; Li, Xiu-Zhuang; Liu, Guo-Yun; Yu, Sha-Sha; Jin, Xiao-Ling; Zhou, Bo
Chemistry - A European Journal, 2012 , vol. 18, # 19 p. 5898 - 5905
反应条件
1: acetic anhydride; triethylamine / 6 h / 110 °C 2: quinoline; copper / 3 h / 200 °C / Inert atmosphere View Scheme
参考文献
Xiao, Chun-Fen; Zou, Yong; Du, Jian-Li; Sun, Hong-Yi; Liu, Xian-Ke
Synthetic Communications, 2012 , vol. 42, # 9 p. 1243 - 1258
反应条件
aluminium trichloride in dichloromethane T=20°C; 12 h;
参考文献
Zou, Hong Bin; Dong, Sheng Yi; Zhou, Chang Xin; Hu, Li Hong; Wu, Yi Hang; Li, Hai Bo; Gong, Jing Xu; Sun, Lian Li; Wu, Xiu Mei; Bai, Hua; Fan, Bo Tao; Hao, Xiao Jiang; Stoeckigt, Joachim; Zhao, Yu
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 6 p. 2060 - 2071
反应条件
camphor-10-sulfonic acid in benzene T=40°C; Yield given. Yields of byproduct given;
参考文献
Corey; Chen; Parry
Tetrahedron Letters, 1988 , vol. 29, # 24 p. 2899 - 2902
反应条件
ammonium acetate in ethanol 6 h; Heating;
参考文献
Quermonne; Dallemagne; Louchahi-Raoul; Pilo; Rault; Robba
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 9 p. 961 - 965
