3,4,5-三甲氧基苯甲醛合成路线 （共 427 条）
反应条件
ammonium acetate in butan-1-ol Rodionov reaction; Heating;
参考文献
Lebedev; Lebedeva; Sheludyakov; Kovaleva; Ustinova; Kozhevnikov
Russian Journal of General Chemistry, 2005 , vol. 75, # 7 p. 1113 - 1124
反应条件
1.1: [3H]-L-Alanine; pyridine / 1.5 h / |Reflux 1.2: 1 h / 20 °C 2.1: sodium hydroxide / methanol / 16 h / 20 °C 3.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C 4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 0.5 h / 20 °C 4.2: 24 h / 20 °C View Scheme
参考文献
Jung, Jae-Chul; Min, Dongguk; Lim, Heena; Moon, Sohyeon; Jung, Mankil; Oh, Seikwan
Medicinal Chemistry Research, 2013 , vol. 22, # 10 p. 4615 - 4621
反应条件
sodium hydroxide in ethanol
参考文献
Al-Omary, Fatmah A.M.; Hassan, Ghada S.; El-Messery, Shahenda M.; El-Subbagh, Hussein I.
European Journal of Medicinal Chemistry, 2012 , vol. 47, # 1 p. 65 - 72
反应条件
ammonium acetate T=20°C; 0.75 h; Neat (no solvent);
参考文献
Datta, Bandita; Pasha, M. Afzal
Chinese Journal of Catalysis, 2011 , vol. 32, # 6-8 p. 1180 - 1184
反应条件
1: With cellulose sulfuric acid in neat (no solvent) T=80 - 100°C; Hantzsch Pyridine Synthesis; 2: With cellulose sulfuric acid in neat (no solvent) Hantzsch Pyridine Synthesis;
参考文献
Murthy; Rajack, Abdul; Taraka Ramji; Jeson Babu; Praveen, Ch.; Aruna Lakshmi
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 18 p. 6016 - 6023
反应条件
bromine in chloroform; water Heating / reflux;
参考文献
Labruere, Raphael; Helissey, Philippe; Desbene-Finck, Stephanie; Giorgi-Renault, Sylviane
Letters in Organic Chemistry, 2012 , vol. 9, # 8 p. 568 - 571,4
反应条件
N-bromosuccinmide in tetrachloromethane Bromination; 12 h; Irradiation;
参考文献
Sarma, Jagarlapudi A.R.P.; Nagaraju, Akula; Majumdar, Kanak K.; Samuel, Purnima M.; Das, Indira; Roy, Sujit; McGhie, Alistair J.
Journal of the Chemical Society. Perkin Transactions 2, 2000 , # 6 p. 1119 - 1123
参考文献
Merchant,J.R. et al.
Journal of the Indian Chemical Society, 1971 , vol. 48, p. 483 - 489
反应条件
1: T=0 - 20°C; 8 h; Inert atmosphere; 2: With water in diethyl ether Inert atmosphere;
参考文献
Tanpure, Rajendra P.; Harkrider, Amanda R.; Strecker, Tracy E.; Hamel, Ernest; Trawick, Mary Lynn; Pinney, Kevin G.
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 19 p. 6993 - 7001
反应条件
in diethyl ether T=0 - 5°C; Grignard reaction; 2 h;
参考文献
Koul, Surrinder; Koul, Jawahir L.; Taneja, Subhash C.; Dhar, Kanaya L.; Jamwal, Deshvir S.; Singh, Kuldeep; Reen, Rashmeet K.; Singh, Jaswant
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 1 p. 251 - 268
