5-疏基-1-苯基-四氮唑合成路线 （共 82 条）
反应条件
triethylamine in ethyl acetate T=0°C; 6 h;
参考文献
Takeda, Kazuyoshi; Tsuboyama, Kanoko; Takayanagi, Hiroaki; Ogura, Haruo
Synthesis, 1987 , # 6 p. 560 - 562
反应条件
triethylamine in ethyl acetate T=0°C; 6 h;
参考文献
Takeda, Kazuyoshi; Tsuboyama, Kanoko; Takayanagi, Hiroaki; Shirokami, Rie; Takeura, Masumi; Ogura, Haruo
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 9 p. 2334 - 2337
反应条件
sodium acetate in water; acetonitrile T=25°C; Electrolysis;
参考文献
Khodaei, Mohammad M.; Alizadeh, Abdolhamid; Pakravan, Narges
Journal of Organic Chemistry, 2008 , vol. 73, # 7 p. 2527 - 2532
反应条件
1: With acetic acid Inert atmosphere; 2: With mercury(II) diacetate Inert atmosphere; 3: With iodine; potassium iodide Inert atmosphere;
参考文献
Balsanek, Vojtech; Tichotova, Lucie; Kunes, Jiri; Spulak, Marcel; Pour, Milan; Votruba, Ivan; Buchta, Vladimir
Collection of Czechoslovak Chemical Communications, 2009 , vol. 74, # 7-8 p. 1161 - 1178
反应条件
1: 47.6 percent / sodium ethoxide / ethanol / 1 h / Heating 2: 76.6 percent / aq. NH3 / ethanol / 2 h View Scheme
参考文献
Waisser, Karel; Vanzura, Jiri; Hrabalek, Alexandr; Vinsova, Jarmila; Gresak, Stefan; et al.
Collection of Czechoslovak Chemical Communications, 1991 , vol. 56, # 11.1 p. 2389 - 2394
反应条件
sodium hydroxide; tetrabutylammomium bromide in chloroform
T=60°C; Alkylation; 7 h;
参考文献
Gol'tsberg; Koldobskii
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 8 p. 1194 - 1201
反应条件
sodium hydroxide
T=20°C; 12 h;
参考文献
Golomolzin, B. V.; Tarakhtii, E. A.; Tregubenko, I. P.; Ryazanova, G. A.; Sidel'kovskaya, F. P.; et al.
Pharmaceutical Chemistry Journal, 1988 , vol. 22, # 7 p. 563 - 567
Khimiko-Farmatsevticheskii Zhurnal, 1988 , vol. 22, # 7 p. 839 - 843
反应条件
potassium carbonate in acetone
3 h; Heating;
参考文献
Uchida; Komatsu; Morita; Kanbe; Yamasaki; Nakagawa
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 4 p. 958 - 961
反应条件
1,1,1,3,3,3-hexamethyl-disilazane in 1,2-dichloro-ethane
参考文献
Gist-Brocades N.V.
Patent: US4379923 A1, 1983 ;
反应条件
1: 92 percent / anhydrous potassium carbonate / acetone / 19 h / 20 - 40 °C
2: 81 percent / hydrogen peroxide; ammonium heptamolybdate(VI) tetrahydrate / tetrahydrofuran; various solvent(s) / 20 °C
View Scheme
参考文献
Al Dulayymi, Juma'a R.; Baird, Mark S.; Roberts, Evan; Minnikin, David E.
Tetrahedron, 2006 , vol. 62, # 51 p. 11867 - 11880
