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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
86005-12-1
合成路线
（共 14 条）
188525-93-1
→
反应条件
86005-12-1
反应条件
carbon tetrabromide; triphenylphosphine in dichloromethane T=0 - 20°C;
参考文献
Sun, Chong-Qing; Cheng, Peter T.W.; Stevenson, Jay; Dejneka, Tamara; Brown, Baerbel; Wang, Tammy C.; Robl, Jeffrey A.; Poss, Michael A.
Tetrahedron Letters, 2002 , vol. 43, # 7 p. 1161 - 1164
75-44-5
光气
+
52279-28-4
→
反应条件
86005-12-1
反应条件
pyridine; p-TsOH; sodium hydrogencarbonate in toluene; benzene
参考文献
E. I. Du Pont de Nemours and Company
Patent: US5310929 A1, 1994 ;
US 5310929 A
86005-11-0
+
94-36-0
过氧化苯甲酰
→
反应条件
86005-12-1
反应条件
N-bromosuccinmide in tetrachloromethane
参考文献
Merck and Co., Inc.
Patent: US4479947 A1, 1984 ;
86005-11-0
→
反应条件
86005-12-1
反应条件
N-bromosuccinmide; azobisisobutyronitrile in tetrachloromethane 1 h; Heating;
参考文献
Sakamoto; Ikeda; Tsukamoto
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 6 p. 2241 - 2248
77902-92-2
→
反应条件
86005-12-1
反应条件
1.1: p-toluenesulfonylazide; Et3N / acetonitrile / 0 - 20 °C 2.1: Rh2(OAc)4 / tetrahydrofuran; H2O / Heating 3.1: i-Pr2NEt / tetrahydrofuran / 0 °C 4.1: hydrogen / Pd(OH)2 on carbon / ethanol / 760 Torr 5.1: oxalyl chloride; DMF / CH2Cl2 / 0 - 20 °C 5.2: Bu4NBH4 / CH2Cl2 / -78 °C 6.1: 84 percent / CBr4; Ph3P / CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Sun, Chong-Qing; Cheng, Peter T.W.; Stevenson, Jay; Dejneka, Tamara; Brown, Baerbel; Wang, Tammy C.; Robl, Jeffrey A.; Poss, Michael A.
Tetrahedron Letters, 2002 , vol. 43, # 7 p. 1161 - 1164
188526-15-0
→
反应条件
86005-12-1
反应条件
1.1: i-Pr2NEt / tetrahydrofuran / 0 °C 2.1: hydrogen / Pd(OH)2 on carbon / ethanol / 760 Torr 3.1: oxalyl chloride; DMF / CH2Cl2 / 0 - 20 °C 3.2: Bu4NBH4 / CH2Cl2 / -78 °C 4.1: 84 percent / CBr4; Ph3P / CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Sun, Chong-Qing; Cheng, Peter T.W.; Stevenson, Jay; Dejneka, Tamara; Brown, Baerbel; Wang, Tammy C.; Robl, Jeffrey A.; Poss, Michael A.
Tetrahedron Letters, 2002 , vol. 43, # 7 p. 1161 - 1164
188526-14-9
→
反应条件
86005-12-1
反应条件
1.1: Rh2(OAc)4 / tetrahydrofuran; H2O / Heating 2.1: i-Pr2NEt / tetrahydrofuran / 0 °C 3.1: hydrogen / Pd(OH)2 on carbon / ethanol / 760 Torr 4.1: oxalyl chloride; DMF / CH2Cl2 / 0 - 20 °C 4.2: Bu4NBH4 / CH2Cl2 / -78 °C 5.1: 84 percent / CBr4; Ph3P / CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Sun, Chong-Qing; Cheng, Peter T.W.; Stevenson, Jay; Dejneka, Tamara; Brown, Baerbel; Wang, Tammy C.; Robl, Jeffrey A.; Poss, Michael A.
Tetrahedron Letters, 2002 , vol. 43, # 7 p. 1161 - 1164
188526-16-1
→
反应条件
86005-12-1
反应条件
1.1: hydrogen / Pd(OH)2 on carbon / ethanol / 760 Torr 2.1: oxalyl chloride; DMF / CH2Cl2 / 0 - 20 °C 2.2: Bu4NBH4 / CH2Cl2 / -78 °C 3.1: 84 percent / CBr4; Ph3P / CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Sun, Chong-Qing; Cheng, Peter T.W.; Stevenson, Jay; Dejneka, Tamara; Brown, Baerbel; Wang, Tammy C.; Robl, Jeffrey A.; Poss, Michael A.
Tetrahedron Letters, 2002 , vol. 43, # 7 p. 1161 - 1164
17094-34-7
特戊酰基乙酸乙酯
→
反应条件
86005-12-1
反应条件
1.1: DMAP / toluene / Heating 2.1: p-toluenesulfonylazide; Et3N / acetonitrile / 0 - 20 °C 3.1: Rh2(OAc)4 / tetrahydrofuran; H2O / Heating 4.1: i-Pr2NEt / tetrahydrofuran / 0 °C 5.1: hydrogen / Pd(OH)2 on carbon / ethanol / 760 Torr 6.1: oxalyl chloride; DMF / CH2Cl2 / 0 - 20 °C 6.2: Bu4NBH4 / CH2Cl2 / -78 °C 7.1: 84 percent / CBr4; Ph3P / CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Sun, Chong-Qing; Cheng, Peter T.W.; Stevenson, Jay; Dejneka, Tamara; Brown, Baerbel; Wang, Tammy C.; Robl, Jeffrey A.; Poss, Michael A.
Tetrahedron Letters, 2002 , vol. 43, # 7 p. 1161 - 1164
3282-30-2
三甲基乙酰氯
→
反应条件
86005-12-1
反应条件
1.1: MgCl2; Et3N / acetonitrile 2.1: DMAP / toluene / Heating 3.1: p-toluenesulfonylazide; Et3N / acetonitrile / 0 - 20 °C 4.1: Rh2(OAc)4 / tetrahydrofuran; H2O / Heating 5.1: i-Pr2NEt / tetrahydrofuran / 0 °C 6.1: hydrogen / Pd(OH)2 on carbon / ethanol / 760 Torr 7.1: oxalyl chloride; DMF / CH2Cl2 / 0 - 20 °C 7.2: Bu4NBH4 / CH2Cl2 / -78 °C 8.1: 84 percent / CBr4; Ph3P / CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Sun, Chong-Qing; Cheng, Peter T.W.; Stevenson, Jay; Dejneka, Tamara; Brown, Baerbel; Wang, Tammy C.; Robl, Jeffrey A.; Poss, Michael A.
Tetrahedron Letters, 2002 , vol. 43, # 7 p. 1161 - 1164
1
2
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