5-硝基-1-苯并噻吩-2-羰酰氯合成路线 （共 8 条）
反应条件
phosphorus pentachloride
参考文献
Justus Liebigs Annalen der Chemie, , vol. 527, p. 83,101
反应条件
1: 45 percent / aq. NaOH / ethanol / 6 h / Heating 2: 70 percent / sodium carbonate; thionyl chloride / toluene / 4 h / Heating View Scheme
参考文献
Egyptian Journal of Chemistry, , vol. 46, # 5 p. 757 - 768
反应条件
1: Na2S; Na2CO3; aqueous ethanol / Erhitzen der Reaktionsloesung mit wss.Natrium-chloracetat-Loesung 2: aq. NaOH solution 3: phosphorus (V)-chloride View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 527, p. 83,101
反应条件
1: aq. NaOH solution 2: phosphorus (V)-chloride View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 527, p. 83,101
反应条件
1: benzene
2: aq. N2H4 / Raney-Ni / ethanol / Heating
View Scheme
参考文献
Lewis,J.J. et al.
Journal of Medicinal Chemistry, 1963 , vol. 6, p. 711 - 716
参考文献
Lewis,J.J. et al.
Journal of Medicinal Chemistry, 1963 , vol. 6, p. 711 - 716
反应条件
1: benzene
2: aq. N2H4 / Raney-Ni / ethanol / Heating
3: LiAlH4 / tetrahydrofuran / Heating
View Scheme
参考文献
Lewis,J.J. et al.
Journal of Medicinal Chemistry, 1963 , vol. 6, p. 711 - 716
反应条件
1: 5.94 g / NaBH4 / dioxane / 0.08 h / Heating
2: 96 percent / t-butyl chromate / 2-methyl-propan-2-ol
View Scheme
参考文献
Zayed; Attia
Journal of Heterocyclic Chemistry, 1983 , vol. 20, # 1 p. 129 - 131
