in benzene byproducts: Si(CH3)3P(C6H5)2; SiMe3Cl added to soln. of complex in C6H6 at room temp.; solvent removed, residue washed with n-hexane to give complex;

in benzene byproducts: P(C6H5)2P(C6H5)2; PPh2Cl injected into soln. of complex, stirred for 3 min at room temp.; solv. removed in vac., solid extd. with n-hexane to leave Zr complex;

in benzene byproducts: P(C6H5)2P(C6H5)2; AsPh2Cl injected into soln. of complex, stirred for 3 min at room temp.; solv. removed in vac., solid extd. with n-hexane to leave Zr complex;

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