1,3-二噻戊环-2-基甲醇合成路线 (共 3 条)
反应条件
methanol; sodium tetrahydroborate in diethyl ether
T=20°C; Reduction; 0.25 h;
参考文献
Khanapure, Subhash P.; Saha, Goutam; Sivendran, Sashikala; Powell, William S.; Rokach, Joshua
Tetrahedron Letters, 2000 , vol. 41, # 30 p. 5653 - 5657
反应条件
potassium hydroxide in ethanol; water
12 h; Ambient temperature;
参考文献
Aparicio, F. J. Lopez; Benitez, F. Zorrilla; Gonzalez, F. Santoyo
Carbohydrate Research, 1983 , vol. 114, p. 287 - 296
反应条件
titanium(IV) isopropylate; alpha,alpha-dimethylbenzyl hydroperoxide; (+)-Weinsaeure-diethylester
1.) CH2Cl2, -38 deg C, 1 h, 2.) CH2Cl2, -38 deg C, 30 min then -30 deg C, 40 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Aggarwal, Varinder K.; Gueltekin, Zeynep; Grainger, Richard S.; Adams, Harry; Spargo, Peter L.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 17 p. 2771 - 2781