4-甲基-7-(2-氧代环己基氧基)-色烯-2-酮合成路线 （共 7 条）
反应条件
1: aq. NaOH / Heating 2: DDQ / toluene / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 49, # 3 p. 1149 - 1156
反应条件
potassium carbonate; potassium iodide in acetone
Heating;
参考文献
Shen, Qiong; Peng, Quan; Shao, Jialiang; Liu, Xufeng; Huang, Zhishu; Pu, Xianzhang; Ma, Lin; Li, Yue-Ming; Chan, Albert S.C.; Gu, Lianquan
European Journal of Medicinal Chemistry, 2005 , vol. 40, # 12 p. 1307 - 1315
反应条件
potassium carbonate in acetone
20 h; Heating;
参考文献
Rodighiero; Palumbo; Magno; et al.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 5 p. 1405 - 1410
反应条件
1: 80 percent / H2SO4 / 0 - 5 °C
2: 80 percent / K2CO3; KI / acetone / Heating
View Scheme
参考文献
Shen, Qiong; Peng, Quan; Shao, Jialiang; Liu, Xufeng; Huang, Zhishu; Pu, Xianzhang; Ma, Lin; Li, Yue-Ming; Chan, Albert S.C.; Gu, Lianquan
European Journal of Medicinal Chemistry, 2005 , vol. 40, # 12 p. 1307 - 1315
反应条件
sodium hydroxide in methanol; water
Heating;
参考文献
Kelkar, Shriniwas L.; Patil, Sharadbala D.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 1 p. 91 - 92
反应条件
sodium hydroxide
Heating;
参考文献
Rodighiero; Palumbo; Magno; et al.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 5 p. 1405 - 1410
反应条件
1: 95 percent / aq. NaOH / 3 h / Heating
2: 98 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / Pd/C / toluene / 6 h / Heating
3: 90 percent / SeO2 / xylene / 24 h / Heating
View Scheme
参考文献
Shen, Qiong; Peng, Quan; Shao, Jialiang; Liu, Xufeng; Huang, Zhishu; Pu, Xianzhang; Ma, Lin; Li, Yue-Ming; Chan, Albert S.C.; Gu, Lianquan
European Journal of Medicinal Chemistry, 2005 , vol. 40, # 12 p. 1307 - 1315
